Reference : Validation of a fast gas chromatographic method for the study of semiochemical slow r...
Scientific journals : Article
Life sciences : Entomology & pest control
Physical, chemical, mathematical & earth Sciences : Chemistry
http://hdl.handle.net/2268/71663
Validation of a fast gas chromatographic method for the study of semiochemical slow release formulations
English
Rozet, Eric mailto [Université de Liège - ULg > Département de pharmacie > Chimie analytique >]
Heuskin, Stéphanie mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie analytique >]
Lorge, Stéphanie [> >]
Farmakidis, Julien [Université de Liège - ULg > Sciences agronomiques > Entomologie fonctionnelle et évolutive >]
Hubert, Philippe mailto [Université de Liège - ULg > Département de pharmacie > Chimie analytique >]
Verheggen, François mailto [Université de Liège - ULg > Sciences agronomiques > Entomologie fonctionnelle et évolutive >]
Haubruge, Eric mailto [Université de Liège - ULg > Services administratifs généraux > Vice-Recteur de Gembloux Agro Bio Tech - Entomologie fonctionnelle et évolutive >]
Wathelet, Jean-Paul mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie générale et organique >]
Lognay, Georges mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie analytique >]
2010
Journal of Pharmaceutical & Biomedical Analysis
Elsevier Science
53
962-972
Yes (verified by ORBi)
International
0731-7085
Oxford
United Kingdom
[en] validation ; accuracy profile ; sesquiterpenes ; alginate beads ; semiochemicals
[en] The validation of a fast GC-FID analytical method for the quantitative determination of semiochemical sesquiterpenes (E-β-farnesene and β-caryophyllene) to be used in an integrated pest management approach is described. Accuracy profiles using total error as decision criteria for validation were used to verify the overall accuracy of the method results within a well defined range of concentrations and to determine the lowest limit of quantification for each analyte. Furthermore it allowed to select a very simple and reliable regression model for calibration curve for the quantification of both analytes as well as to provide measurement uncertainty without any additional experiments.
Finally, this validated method was used for the quantification of semiochemicals in slow release formulations. The goal was to verify the protection efficiency of alginate gel beads formulations against oxidation and degradation of sesquiterpenes. The results showed that the alginate beads are adequate slow release devices which protect the bio-active molecules during at least twenty days.
Researchers ; Professionals ; Students
http://hdl.handle.net/2268/71663
10.1016/j.jpba.2010.07.014

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