ORBi: Brasseur Catherine - Validation of the analytical procedure for the determination of polyaromatic hydrocarbons in smoke flavourings using high performance liquid chromatography coupled to an ultraviolet, diode array or fluorescence detector

Reference : Validation of the analytical procedure for the determination of polyaromatic hydrocarbon...


	Document type :	Scientific journals : Article
	Discipline(s) :	Engineering, computing & technology : Multidisciplinary, general & others Physical, chemical, mathematical & earth Sciences : Chemistry
	To cite this reference:	http://hdl.handle.net/2268/2448

Title :	Validation of the analytical procedure for the determination of polyaromatic hydrocarbons in smoke flavourings using high performance liquid chromatography coupled to an ultraviolet, diode array or fluorescence detector
Language :	English
Author, co-author :	Brasseur, Catherine [Université de Liège - ULg > Département de sciences des denrées alimentaires > Analyse des denrées alimentaires]
	Brose, François [Université de Liège - ULg > Département de sciences des denrées alimentaires > Département de sciences des denrées alimentaires >]
	Pirlot, Alain [Université de Liège - ULg > Département de sciences des denrées alimentaires > Technologie des denrées alimentaires > > >]
	Douny, Caroline [Université de Liège - ULg > Département de sciences des denrées alimentaires > Analyse des denrées alimentaires >]
	Eppe, Gauthier [Université de Liège - ULg > > Centre interfac. d'analyse des résidus en traces (CART) >]
	Maghuin-Rogister, Guy [Université de Liège - ULg > Département de sciences des denrées alimentaires > Département de sciences des denrées alimentaires >]
	Scippo, Marie-Louise [Université de Liège - ULg > Département de sciences des denrées alimentaires > Analyse des denrées alimentaires >]
Publication date :	2007
Journal title :	Accreditation and Quality Assurance
Publisher :	Springer
Volume :	12
Issue/season :	10
Pages :	535-542
Audience :	International
ISSN :	0949-1775
City :	New York
Keywords :	[en] polyaromatic hydrocarbons ; PAH ; HPLC ; UV ; FLD ; smoke flavouring ; analytical procedure validation ; accuracy profile ; uncertainty measurement
Abstract :	[en] High performance liquid chromatography (HPLC) coupled to an ultraviolet (UV), diode array or fluorescence detector (UV/DAD/FLD) has been used to set up an analytical procedure for the quantification of 16 EU priority polyaromatic hydrocarbons (PAHs) in smoke flavourings. The following parameters have been determined for the 16 EU priority PAHs: limit of detection, limit of quantification, precision (repeatability and intermediate precision), recovery and measurement uncertainty, using the concept of accuracy profiles. They were in close agreement with quality criteria described in the Commission Regulation (EC) no. 627/2006 concerning PAHs in smoke flavourings.
Permalink :	http://hdl.handle.net/2268/2448

File(s) associated to this reference

Fulltext file(s):

	File	Commentary	Version	Size	Access
Restricted access	pah_acqual.pdf		Publisher postprint	493.7 kB	Request copy

All documents in ORBi are protected by a user license.

Dspace v1.5