Preparation and evaluation of a novel monolithic column containing double octadecyl chains for reverse-phase micro high performance liquid chromatography.

Duan, Qianqian; Liu, Chusheng; Liu, Zhenghua; Zhou, Zhengyin; Chen, Weijia; Wang, Qiqin; Crommen, Jacques; Jiang, Zhengjin

doi:10.1016/j.chroma.2014.04.036

Article (Scientific journals)

Preparation and evaluation of a novel monolithic column containing double octadecyl chains for reverse-phase micro high performance liquid chromatography.

Duan, Qianqian; Liu, Chusheng; Liu, Zhenghua et al.

2014 • In Journal of Chromatography. A, 1345, p. 174-81

Peer Reviewed verified by ORBi

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https://hdl.handle.net/2268/187181

DOI
10.1016/j.chroma.2014.04.036

PubMed
24786656

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Keywords :

Animals; Chickens; Chromatography, High Pressure Liquid/instrumentation; Chromatography, Reverse-Phase/instrumentation; Cytochromes c/isolation & purification; Ethylene Glycols/chemistry; Methacrylates/chemistry; Microscopy, Electron, Scanning; Muramidase/isolation & purification; Polycyclic Hydrocarbons, Aromatic/isolation & purification; Reproducibility of Results; Ribonucleases/isolation & purification; Tocopherols/isolation & purification; Double alkyl chains; Micro-HPLC; Monoliths; Reverse-phase liquid chromatography

Abstract :

[en] A novel reverse-phase monolithic stationary phase containing double long alkyl chains was prepared based on the thermally initiated co-polymerization of 3-methylacryloyl-3-oxapropyl-3-(N,N-dioctadecylcarbamoyl)-propionate (AOD) and ethylene glycol dimethacrylate (EDMA) in the presence of 2-methyl-1-propanol and 1,4-butanediol as the selected porogens. The polymerization was carefully optimized and good permeability, stability and column efficiency were observed for the final monolithic columns. The column also showed good long term stability and reproducibility. The methylene selectivity demonstrates typical reversed phase characteristics. The optimized poly (AOD-co-EDMA) monolith exhibited good selectivity for a range of non-polar test analytes such as PAHs, tocopherols and alkylphenones. A good separation of intact proteins was also observed.

Research center :

Centre Interfacultaire de Recherche du Médicament - CIRM

Disciplines :

Pharmacy, pharmacology & toxicology

Author, co-author :

Duan, Qianqian

Liu, Chusheng

Liu, Zhenghua

Zhou, Zhengyin

Chen, Weijia

Wang, Qiqin

Crommen, Jacques ; Université de Liège > Département de pharmacie > Département de pharmacie

Jiang, Zhengjin

Language :

English

Title :

Preparation and evaluation of a novel monolithic column containing double octadecyl chains for reverse-phase micro high performance liquid chromatography.

Publication date :

2014

Journal title :

Journal of Chromatography. A

ISSN :

0021-9673

eISSN :

1873-3778

Publisher :

Elsevier, Amsterdam, Netherlands

Volume :

1345

Pages :

174-81

Peer reviewed :

Peer Reviewed verified by ORBi

Commentary :

Available on ORBi :

since 24 October 2015

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