Reference : Fast Clean-up for Polychlorinated Dibenzo-P-Dioxins, Dibenzofurans and Coplanar Polyc...
Scientific journals : Article
Physical, chemical, mathematical & earth Sciences : Chemistry
Life sciences : Food science
http://hdl.handle.net/2268/18685
Fast Clean-up for Polychlorinated Dibenzo-P-Dioxins, Dibenzofurans and Coplanar Polychlorinated Biphenyls Analysis of High-Fat-Content Biological Samples
English
Focant, Jean-François mailto [Université de Liège - ULg > Département de chimie (sciences) > Chimie analytique]
Eppe, Gauthier mailto [Université de Liège - ULg > > Centre interfac. d'analyse des résidus en traces (CART) >]
Pirard, Catherine [ > > ]
De Pauw, Edwin mailto [Université de Liège - ULg > > Chimie physique, spectrométrie de masse >]
3-Aug-2001
Journal of Chromatography. A
925
1-2
207-21
Yes (verified by ORBi)
International
0021-9673
[en] A fast clean-up procedure for the low level analysis of polychlorinated dibenzo-p-dioxins. polychlorinated dibenzofurans and coplanar polychlorinated biphenyls in highly fatty biological matrices using high capacity disposable multi-layer silica columns is presented. Results were compared with gel permeation chromatography for removal of lipids. Analytical criteria such as recovery rates, repeatability, reproducibility and robustness are evaluated through a broad range of biological matrices and reference materials analysis. The final proposed procedure for the complete analysis, including pressurized liquid extraction, Power-Prep system clean-up and GC-high-resolution MS analysis requires only 48 h, and allows the simultaneous preparation of up to 10 samples.
http://hdl.handle.net/2268/18685

File(s) associated to this reference

Fulltext file(s):

FileCommentaryVersionSizeAccess
Restricted access
Focant et al.pdfPublisher postprint613.12 kBRequest copy

Bookmark and Share SFX Query

All documents in ORBi are protected by a user license.