Article (Scientific journals)
Microwave-assisted synthesis of D-glucuronic acid derivatives using cost-effective solid acid catalysts
Richel, Aurore; Laurent, Pascal; Wathelet, Bernard et al.
2010In Tetrahedron Letters, 51, p. 1356-1360
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Keywords :
Microwave chemistry; Carbohydrates; Heterogeneous Catalysis; Silica; Supported Catalysts
Abstract :
[en] Monomode microwave-assisted coupling of D-glucuronic acid with alcohols, in the presence of various impregnated acid catalysts, was successfully performed, affording in almost quantitative yields the corresponding monosubstituted b-D-glucofuranosidurono-6,3-lactones in less than 10 min at 85°C. This study evidences the synergy of microwaves and impregnated acid catalysts as a fast and clean strategy in the field of carbohydrate chemistry.
Disciplines :
Chemistry
Author, co-author :
Richel, Aurore  ;  Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
Laurent, Pascal ;  Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
Wathelet, Bernard ;  Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
Wathelet, Jean-Paul ;  Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
Paquot, Michel ;  Université de Liège - ULiège > Gembloux Agro-Bio Tech > Gembloux Agro-Bio Tech
Language :
English
Title :
Microwave-assisted synthesis of D-glucuronic acid derivatives using cost-effective solid acid catalysts
Publication date :
2010
Journal title :
Tetrahedron Letters
ISSN :
0040-4039
Publisher :
Elsevier, Oxford, United Kingdom
Volume :
51
Pages :
1356-1360
Peer reviewed :
Peer Reviewed verified by ORBi
Name of the research project :
Programme d'Excellence TECHNOSE
Funders :
DGTRE - Région wallonne. Direction générale des Technologies, de la Recherche et de l'Énergie [BE]
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