Reference : Efficient microwave-promoted synthesis of glucuronic and galacturonic acid derivative...
Scientific journals : Article
Physical, chemical, mathematical & earth Sciences : Chemistry
http://hdl.handle.net/2268/103908
Efficient microwave-promoted synthesis of glucuronic and galacturonic acid derivatives using sulfuric acid impregnated on silica
English
Richel, Aurore mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie biologique industrielle >]
Nicks, Francois [Université de Liège - ULg > Chimie et bio-industries > Chimie générale et organique >]
Laurent, Pascal mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie biologique industrielle >]
Wathelet, Bernard mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie biologique industrielle >]
Wathelet, Jean-Paul mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie générale et organique >]
Paquot, Michel mailto [Université de Liège - ULg > Chimie et bio-industries > Chimie biologique industrielle >]
2012
Green Chemistry Letters & Reviews
Taylor & Francis Ltd
5
2
179-186
Yes (verified by ORBi)
International
1751-7192
[en] Microwave chemistry ; Carbohydrates ; Heterogeneous catalysis ; Silica ; Supported catalysts
[en] Monomode microwave-assisted syntheses of D-glucuronic and D-galacturonic acid derivatives are reported in the presence of a solid acid catalyst, consisting of sulfuric acid loaded onto silica. This approach affords a variety of surface-active monoglycosylated glucofuranosidurono-6,3-lactones and disubstituted galacturonic adducts in excellent yields in less than 10 min at 85 °C. This study illustrates the application of microwave heating mode, in combination with a cost-effective solid catalyst, as an efficient, selective and eco-friendly methodology in carbohydrate chemistry.
Région wallonne : Direction générale des Technologies, de la Recherche et de l'Energie - DGTRE
TECHNOSE (Bioraffinerie végétale: chimie et technologie des structures osidiques)
http://hdl.handle.net/2268/103908

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