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See detailFast multiresponsive micellar gels from a smart ABC triblock copolymer
Willet, Nicolas ULg; Gohy, Jean-François; Lei, Liangcai et al

in Angewandte Chemie (International ed. in English) (2007), 46(42), 7988-7992

The triblock copolymer PS-b-P2VP-b-PEO undergoes simultaneous micellization and gelation, leading to high-storage-modulus materials that have fast responses to pH value, temperature, ionic strength, and ... [more ▼]

The triblock copolymer PS-b-P2VP-b-PEO undergoes simultaneous micellization and gelation, leading to high-storage-modulus materials that have fast responses to pH value, temperature, ionic strength, and shearing. The gel has a hierarchical structure with spherical core-shell-corona micelles, which, in turn, pack closely into an ordered cubic structure. [less ▲]

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See detailA Fast Newton-Raphson Method in Stochastic Linearization
Canor, Thomas ULg; Blaise, Nicolas ULg; Denoël, Vincent ULg

in Proceedings of the Ninth International Conference on Structural Dynamics (2014)

Owing to its accessible implementation and rapidity, the equivalent linearization has become a common probabilistic approach for the analysis of large-dimension nonlinear structures, as encountered in ... [more ▼]

Owing to its accessible implementation and rapidity, the equivalent linearization has become a common probabilistic approach for the analysis of large-dimension nonlinear structures, as encountered in earthquake and wind engineering. It consists in replacing the nonlinear system by an equivalent linear one, by tuning the parameters of the equivalent system, in order to minimize some discrepancy error. Consequently classical analysis tools such as the spectral analysis may be reconditioned to approximate the solution of structures with slight to moderate nonlinearities. The tuning of the equivalent parameters requires the solution of a set of nonlinear algebraic equations involving integrals. It is typically performed with the fixed-point algorithm, which is known to behave poorly in terms of convergence. We therefore advocate for the use and implementation of a Newton-Raphson approach, which behaves much better, even in its dishonest formulation. Unfortunately, this latter option requires the costly construction of a Jacobian matrix. In the approach described in this paper, this issue is answered by introducing a series expansion method that provides a fast and accurate estimation of the residual function (whose solution provides the equivalent parameters) and a fast and approximate estimation of the Jacobian matrix. An illustration demonstrate the good accuracy obtained with the proposed method. [less ▲]

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See detailFast production of highly concentrated reactive [18F] fluoride for aliphatic and aromatic nucleophilic radiolabelling
Aerts, Joël ULg; Voccia, Samuel; Lemaire, Christian ULg et al

in Tetrahedron Letters (2010), 51

The use of a polymeric solid support loaded with a long alkyl chain quaternary ammonium allows the rapid and efficient recovery of cyclotron produced [18F]F- from [18O]water to a low water content organic ... [more ▼]

The use of a polymeric solid support loaded with a long alkyl chain quaternary ammonium allows the rapid and efficient recovery of cyclotron produced [18F]F- from [18O]water to a low water content organic solution compatible with fast nucleophilic labelling of most precursors for PET radiopharmaceuticals in high yield. [less ▲]

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See detailFast Production of Highly Reactive No-Carrier-Added [18F]Fluoride for the Labeling of Radiopharmaceuticals
Lemaire, Christian ULg; Aerts, Joël ULg; Voccia, Samuel et al

in Angewandte Chemie (International ed. in English) (2010), 49

The 18F labeling of radiopharmaceuticals requires nearly anhydrous solutions of [18F]fluoride. Aqueous K2CO3 is generally used to elute [18F]fluoride from an anion-exchange resin. Replacing aqueous K2CO3 ... [more ▼]

The 18F labeling of radiopharmaceuticals requires nearly anhydrous solutions of [18F]fluoride. Aqueous K2CO3 is generally used to elute [18F]fluoride from an anion-exchange resin. Replacing aqueous K2CO3 with strong organic bases, such as the phosphazene base P2Et enabled the recovery of highly reactive [18F]fluoride and avoided the azeotropic evaporation of water, which is very difficult on a microchip device. [less ▲]

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See detailFast quality control of short-lived radiopharmaceutical compounds with a photodiode array detector.
Plenevaux, Alain ULg; Lemaire, Christian ULg; Aerts, Joël ULg et al

in Journal of Labelled Compounds & Radiopharmaceuticals (1995), 37

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See detailThe fast regulation of aromatase activity by phosphorylations is species and tissue-independent.
Charlier, Thierry ULg; Harada, Nobuhiro; Ball, Gregory F. et al

Poster (2009)

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See detailFast routine production of L-[11C-methyl]methionine with Al2O3/KF in a disposable unit.
Del Fiore, G.; Schmitz, F.; Plenevaux, Alain ULg et al

in Journal of Labelled Compounds & Radiopharmaceuticals (1995), 37

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See detailFast Routine Production of L-[11C-methyl]methionine with Al2O3KF
Schmitz, Frédéric; Plenevaux, Alain ULg; Del-Fiore, Guy et al

in Applied Radiation & Isotopes (1995), 46(9), 893-897

No-carrier-added (nca) L-[11C-methyl]methionine was prepared via the very fast S-alkylation of L-homocysteine adsorbed on AI203/KF with [11C]iodomethane at room temperature in ethanol. The alkylation was ... [more ▼]

No-carrier-added (nca) L-[11C-methyl]methionine was prepared via the very fast S-alkylation of L-homocysteine adsorbed on AI203/KF with [11C]iodomethane at room temperature in ethanol. The alkylation was realized with a radiochemical yield of 94 +/- 4% EOB (n = 20). More than 90% (n = 20) of the precursor L-homocysteine remained adsorbed on the solid support and was eliminated by a simple filtration. After reaction, neither racemization nor by-product were detected. The purification process was thus limited to a C18 Sep-Pak followed by an alumina Sep-Pak. The radiochemical purity measured on the final solution was shown to be > 99%. The only chemical contaminant was L-homocysteine (+ 10 µg). With this new technique, L-[11C-methyl]methionine was ready for injection within 10 min from [11C]CO2 with a specific activity ranging around 37 + 5.6 GBq (1 +/- 0.15 Ci)//tmol EOB. Through this procedure L-[11C-methyl]methionine can be prepared without preparative HPLC purification, This is an important simplification for the fast routine production of one of the most widely used radiopharmaceutical compounds for PET. [less ▲]

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See detailFast small-disturbance analysis of long-term voltage stability
Rousseaux, Patricia ULg; Van Cutsem, Thierry ULg

in Proceedings of the 12th Power System Computation Conference (PSCC) (1996)

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See detailFast Strength Assessment of Mitre Gates to Ship Impact
Buldgen, Loïc ULg; Le Sourne, Hervé; Rigo, Philippe ULg

in International Journal of Crashworthiness (2013)

Fast Strength Assessment of Mitre Gates to Ship Impact

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See detailFast transient stability assessment revisited
Toumi, B.; Dhifaoui, R.; Van Cutsem, Thierry ULg et al

in IEEE Transactions on Power Systems (1986), 1

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See detailA Fast Universal Solver for 1D Continuous and Discontinuous Steady Flows in Rivers and Pipes
Kerger, François ULg; Archambeau, Pierre ULg; Erpicum, Sébastien ULg et al

in International Journal for Numerical Methods in Fluids (2011), 66(1), 3343

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See detailFast, sensitive, and comprehensive analytical methods including three-dimensional analysis (GCXGC-TOFMS) for measuring halogenated persistent organic pollutants
Patterson, Donald G.; Turner, Wayman E.; Sjödin, Andreas et al

in Organohalogen Compounds (2003), 60-65

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See detailFast-evolving weather for the coolest of our two new substellar neighbours
Gillon, Michaël ULg; Triaud, A. H. M. J.; Jehin, Emmanuel ULg et al

in Astronomy and Astrophysics (2013), 555

We present the results of an intense photometric monitoring in the near-infrared (~0.9 microns) with the TRAPPIST robotic telescope of the newly discovered binary brown dwarf WISE J104915.57-531906.1, the ... [more ▼]

We present the results of an intense photometric monitoring in the near-infrared (~0.9 microns) with the TRAPPIST robotic telescope of the newly discovered binary brown dwarf WISE J104915.57-531906.1, the third closest system to the Sun at a distance of only 2 pc. Our twelve nights of photometric time-series reveal a quasi-periodic (P = 4.87+-0.01 h) variability with a maximal peak-peak amplitude of ~11% and strong night-to-night evolution. We attribute this variability to the rotational modulation of fast-evolving weather patterns in the atmosphere of the coolest component (~T1-type) of the binary. No periodic signal is detected for the hottest component (~L8-type). For both brown dwarfs, our data allow us to firmly discard any unique transit during our observations for planets >= 2 Rearth. For orbital periods smaller than ~9.5 h, transiting planets are excluded down to an Earth-size. [less ▲]

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See detailFast-GC quantifacation of harmonine, the major defense alkaloid of the multicolored Asian ladybird Harmonia axyridis (Pallas)
Fischer, Christophe ULg; Laurent, Pascal ULg; Heuskin, Stéphanie ULg et al

in American Journal of Analytical Chemistry (2012), 3

These last few years the multicolored Asian ladybird, Harmonia axyridis (Pallas), previously introduced in Europe and North America as a biological control agent, has swiftly spread out on those ... [more ▼]

These last few years the multicolored Asian ladybird, Harmonia axyridis (Pallas), previously introduced in Europe and North America as a biological control agent, has swiftly spread out on those territories and turns out to be a pest in several ways. In order to improve understanding of several key points of the biology of this ladybird, a novel fast-GC method of quantification of harmonine, the main defense alkaloid of H. axyridis, has been designed and validated using the accuracy profile concept for concentrations ranging from 13 to 264 µg/individual. This method allows quantifying harmonine in a single insect with a maximal error risk of 20%. For ladybirds collected in spring, mean harmonine concentration observed was 106.6 µg/individual with a very high standard deviation of 80.2 µg/individual, which can easily be explained by the strong asymmetry of the results distribution. Males and females seem equally chemically protected as the harmonine concentration did not significantly differ between sexes. This method is currently used to improve our comprehension of several key points of H. axyridis biology including aggregation behavior and aposematism. [less ▲]

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See detailFast-GC quantification of harmonine, the major defense alkaloid of the multicolored asian ladybird Harmonia axyridis (Pallas)
Fischer, Christophe ULg; Laurent, P; Heuskin, Stéphanie ULg et al

in American Journal of Analytical Chemistry (2012), 3

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See detailFastes princiers et culte eucharistique au pays de Liège : cérémonies baroques au cœur d’une principauté ecclésiastique des XVIIe et XVIIIe siècles
Henneau, Marie-Elisabeth ULg

in Dompnier, Bernard (Ed.) Les cérémonies extraordinaires du Catholicisme baroque (2009)

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