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See detailDevelopment of a hydrogen maser in the TE111 mode
Van Der Beken, Emeline ULg; Léonard, Daniel; Counet, Arnaud et al

Poster (2016, May 18)

We present the recent progress in the development of a hydrogen maser in the unusual TE111 mode. In contrast to standard hydrogen maser that exploits the TE011 mode, the TE111 mode allows one to design ... [more ▼]

We present the recent progress in the development of a hydrogen maser in the unusual TE111 mode. In contrast to standard hydrogen maser that exploits the TE011 mode, the TE111 mode allows one to design hydrogen masers with significant reduced dimensions which represents a huge benefit for space applications and in particular for the global positioning system. We present in details the different parts of our model : cavity with a thin Teflon sheet, magnetic shielding, temperature control of the maser... [less ▲]

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See detailDevelopment of a LC-MS/MS analytical method for the simultaneous measurement of aldehydes coming from polyunsaturated fatty acids degradation in animal feed
Douny, Caroline ULg; Bayram, Pinar; Brose, François ULg et al

in Drug Testing and Analysis (2016), 8(5-6), 458-464

Knowing that polyunsaturated fatty acids can lead to the formation of potentially toxic aldehydes as secondary oxidation products, an analytical method using liquid chromatography coupled to tandem mass ... [more ▼]

Knowing that polyunsaturated fatty acids can lead to the formation of potentially toxic aldehydes as secondary oxidation products, an analytical method using liquid chromatography coupled to tandem mass spectrometry detection (LC-MS/MS) has been developed to evaluate the concentration of eight aldehydes in animal feed: malondialdehyde (MDA), 4-hydroxy-2-nonenal (4-HNE), 4-hydroxy-2-hexenal (4-HHE), crotonaldehyde (CRT), benzaldehyde (BNZ), hexanal (HXL), 2,4-nonadienal and 2,4-decadienal. The developed method has been validated according to the criteria and procedure described in international standards. The evaluated parameters were: specificity/selectivity, recovery, precision, accuracy, uncertainty, limits of detection and quantification, using the concept of accuracy profiles. These parameters have been determined during experiments realized on 3 different days with grounded Kellogg’s® Corn Flakes® cereals as model matrix for animal feed and spiked at different levels of concentration. Malondialdehyde, 4-HHE, 4-HNE, crotonaldehyde, benzaldehyde and hexanal can be analysed in the same run in animal feed with a very good accuracy, with recovery rates ranging from 86 to 109% for a working range going from 0.16 to 12.50 mg/kg. Concerning 2,4-nonadienal and 2,4-decadienal, their analysis can be realized as well but in a limited range of concentration and with a limited accuracy. Indeed, recovery rates ranged between 54 and 114% and coefficient of variation for the intermediate precision between 11 and 25% for these two compounds. [less ▲]

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See detailDevelopment of a LC-UV-MS analytical method for malondialdehyde.
Douny, Caroline ULg; Dure, Remy; Brose, François ULg et al

Poster (2011)

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See detailDevelopment of a liquid chromatographic method for thesimultaneous quantification of curcumin, -arteether,tetrahydrocurcumin and dihydroartemisinin. Application to lipid-based formulations
Memvanga Bondo, Patrick; Mbinze Kindenge, Jérémie ULg; Rozet, Eric ULg et al

in Journal of Pharmaceutical & Biomedical Analysis (2014), 88

A liquid chromatographic method was developed for the simultaneous separation of curcumin, B-arteether, tetrahydrocurcumin and dihydroartemisinin based on the design of experiments and the design space ... [more ▼]

A liquid chromatographic method was developed for the simultaneous separation of curcumin, B-arteether, tetrahydrocurcumin and dihydroartemisinin based on the design of experiments and the design space methodology. The influence of the percentage of organic modifier, flow rate of the mobile phase and column temperature on the analytes separation was investigated. The optimal chromatographic separation was achieved on a C18 column (125 mm × 4 mm, 5 µm) using an isocratic elution with a mobile phase consisting of methanol:ammonium acetate (pH 4; 10 mM) (80/20, v/v) at a flow rate of 0.45 ml/min and a column temperature of 32.5◦C. This method was then validated for simultaneous quantification of curcumin and B -arteether contained in lipid-based formulations taking into account the B -expectation tolerance interval for the total error measurement. Finally, the suitability of the proposed liquid chromatographic method for routine analysis of curcumin and B -arteether loaded in lipid-based formulations has been proven. [less ▲]

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See detailDevelopment of a long-acting sulfamethazine bolus for sheep
Evrard, Brigitte ULg; Dechesne, Jean-Paul; Fagetton, Xavier et al

in Proceedings of 6th International Conference of Pharmaceutical Technology (1992)

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See detailDevelopment of a low actuation voltage RF MEMS switch
Kiang, Kian Shen; Kraft, Michaël ULg

in Eurosensors XXII (2008, September)

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See detailDevelopment of a low voltage MEMS switch for RF applications
Kiang, Kian Shen; Kraft, Michaël ULg

in Proc. MME 2006 Conference (2006, September)

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See detailDevelopment of a mass spectrometry method for the determination of a melanoma biomarker, 5-S-cysteinyldopa, in human plasma using solid phase extraction for sample clean-up.
Martin, Gaëlle ULg; Chiap, Patrice ULg; Paquet, Philippe ULg et al

in Journal of Chromatography. A (2007), 1156(1-2), 141-8

5-S-cysteinyldopa is a well-known pigment intermediate and analysis of its plasma concentration is interesting for the early diagnosis, as well as for evaluation of treatment and follow-up of malignant ... [more ▼]

5-S-cysteinyldopa is a well-known pigment intermediate and analysis of its plasma concentration is interesting for the early diagnosis, as well as for evaluation of treatment and follow-up of malignant melanoma. A determination method of 5-SCD in human plasma was developed using solid phase extraction (SPE) on disposable cartridges and liquid chromatography electrospray mass spectrometry (LC-ESI-MS-MS). Compound's sensitivity to light and oxidation requires the addition of anti-oxidative agents (AO), to work in acidic media at 4 degrees C and to avoid light exposure of samples since blood collection. Different solid phases involving covalent binding to phenylboronic groups or dual retention mechanisms were evaluated and extraction cartridges containing both hydrophobic and strong cation exchange functionalities were finally selected. The LC separation of 5-SCD from endogenous catecholamines was achieved by gradient elution on a C18 stationary phase. 5-SCD was detected by multiple reaction monitoring (MRM) performed on ES(+) generated ions. Finally, the method was prevalidated in the lower ng/ml range. Good results with respect to accuracy, trueness and precision were obtained. [less ▲]

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See detailDevelopment of a mechanobiological model of bone formation in orthodontic tooth movement
Van Schepdael, A.; Geris, Liesbet ULg; Vander Sloten, Jos

in Proceedings of the European Conference on Mathematical and Theoretical Biology (2008)

Detailed reference viewed: 11 (0 ULg)