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See detail« Détermination et Liberté »
Cormann, Grégory ULg

in Noudelmann, François; Philippe, Gilles (Eds.) Dictionnaire Sartre (2005)

Detailed reference viewed: 66 (5 ULg)
See detailDétermination et production du starter du Mbannick, lait fermenté du Sénégal.
Cornelius, C.; Roblain, D.; Gningue, P. et al

Conference (1994, May)

Detailed reference viewed: 6 (0 ULg)
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See detailDétermination expérimentale de la résistance au feu – Partie 2 – La norme ISO 17025 comme support de la qualité
Dumont, Fabien ULg

Conference given outside the academic context (2009)

La norme ISO 17025 établit les exigences générales concernant la compétence des laboratoires d'étalonnage et d'essai. En illustration de cette norme, ce module présente les démarches - mises en oeuvre au ... [more ▼]

La norme ISO 17025 établit les exigences générales concernant la compétence des laboratoires d'étalonnage et d'essai. En illustration de cette norme, ce module présente les démarches - mises en oeuvre au Laboratoire d'Essai au Feu de l'ULg - spécifiques aux exigences destinées à assurer la qualité des essais et l'exactitude des résultats. [less ▲]

Detailed reference viewed: 37 (9 ULg)
Peer Reviewed
See detaildetermination methods].; Le selenium dans la nature.
Lognay, Georges ULg

in Annales de Gembloux (1981), 87(1),

Detailed reference viewed: 15 (3 ULg)
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See detailDétermination objective de l’hétérogénéité de la classe et variation des réactions à la prestation
Cloes, Marc ULg; Delfosse, Catherine ULg; Piéron, Maurice

in Revue de l'Education Physique (1989), 29(2), 61-70

Dans l'enseignement général et dans l'enseignement des activités physiques, le responsable pédagogique s'adresse à un groupe d'élèves dont les caractéristiques individuelles les diffèrent parfois ... [more ▼]

Dans l'enseignement général et dans l'enseignement des activités physiques, le responsable pédagogique s'adresse à un groupe d'élèves dont les caractéristiques individuelles les diffèrent parfois fortement. Les différences concernent notamment le niveau d'aptitude physique, cognitif et affectif des apprenants. Depuis plusieurs années, plusieurs chercheurs se sont intéressés à la question de savoir si les enseignants modifiaient leurs comportements lorsqu'ils s'adressent à un type d'élèves ou à l'autre. [less ▲]

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See detailDetermination of 3-tert.butylamino-1,2-propanediol enantiomers by LC-MS-MS
Toussaint, B.; Streel, B.; Ceccato, Attilio ULg et al

Poster (2000)

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See detailDetermination of 4-aminophenol in a pharmaceutical formulation using Surface Enhanced Raman scattering: from development to method validation
De Bleye, Charlotte ULg; Dumont, Elodie ULg; Rozet, Eric ULg et al

in Talanta (2013), 116

A Surface Enhanced Raman Scattering (SERS) method able to quantify 4-aminophenol in a pharmaceutical formulation based on acetaminophen, also called paracetamol, was developed and, for the first time ... [more ▼]

A Surface Enhanced Raman Scattering (SERS) method able to quantify 4-aminophenol in a pharmaceutical formulation based on acetaminophen, also called paracetamol, was developed and, for the first time, successfully validated. In this context, silver nanoparticles were synthesized according to the method described by Lee-Meisel and used as SERS substrate. The repeatability of the silver colloid synthesis was tested using different methods to characterise the size and the zeta potential of silver nanoparticles freshly synthesized. To optimize the SERS samples preparation, a design of experiments implicating concentrations of citrate-reduced silver nanoparticles and aggregating agent was performed in order to maximize the Raman signal enhancement. Finally, an approach based on tolerance intervals and accuracy profiles was applied in order to thoroughly validate the method in a range of concentrations comprised from 3 to 15 µg mL-1 using normalized band intensities. The standard addition method was selected as method calibration. Therefore, measurements were carried out on 4-aminophenol spiked solutions of the pharmaceutical formulation. Despite the well-known stability and reproducibility problems of SERS, the validation was performed using two operators and 5 batches of nanoparticles, one for each validation day. [less ▲]

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See detailDetermination of a coalescence parameter from batch-settling experiments
Henschke, M; Schlieper, L; Pfennig, Andreas ULg

in Chemical Engineering Journal (2002), 85((2-3)), 369-378

Detailed reference viewed: 22 (0 ULg)
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See detailDetermination of a gravity and shock score for prognosis in equine surgical colic
Grulke, Sigrid ULg; Olle, E.; Detilleux, Johann ULg et al

in Journal of Veterinary Medicine. A, Physiology, Pathology, Clinical Medicine (2001), 48(8), 465-73

A retrospective study evaluated 200 surgical colic cases. A gravity score (GS) based on four clinical parameters estimating intestinal obstruction (rectal palpation, borborygmi, abdominal distension, pain ... [more ▼]

A retrospective study evaluated 200 surgical colic cases. A gravity score (GS) based on four clinical parameters estimating intestinal obstruction (rectal palpation, borborygmi, abdominal distension, pain) and classified into three categories was established and tested to determine if it could evaluate prognosis. A shock score (SS) based on six parameters was also attributed to each case. The overall survival rate was 54%. The statistical analysis showed a significant (P < 0.01) difference in the survival rate in the different categories of the GS, as well as in the categories of the SS. A multivariate logistic regression model showed that horses with GS 3 are 10.6 times more likely to die than those with GS 1. A model combining the two scores showed an odds ratio of 7.1 for GS 3 versus GS 1, and for SS 3 versus SS 1, the odds ratio was 7.2. [less ▲]

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See detailDetermination of a Suitable Protocol for Indigenous Oilseed Cucurbits Plant Regeneration
Gnamien, Yah Gwladys; Zoro Bi, I. A.; Djè, Y. et al

in Tropicultura (2010), 28(4), 217-225

The present work was carried out to establish rapid in vitro propagation of the indigenous oilseed Citrullus lanatus. Efficiency of 3 protocols for seed decontamination was investigated. High level of ... [more ▼]

The present work was carried out to establish rapid in vitro propagation of the indigenous oilseed Citrullus lanatus. Efficiency of 3 protocols for seed decontamination was investigated. High level of seed sterilization was obtained after removing seed coat and soaking the seeds in 1.6 % sodium hypochlorite with a drop of Tween 20. Shoot tips, single node and cotyledon explants of 3 morphotypes have been screened for adventitious shoot formation in tissue culture. Best response in termis of multiple shoot induction was obtained from cotyledon proximal part with hypocotyl segmenet on Murashige and Skoog medium supplemented with 1 mg/l 6-Benzylaminopurine, 30 g/l sucrose and 8 g/l agar. After 3 weeks of culture, 90% of cotyledon proximal parts induced shoot. An average of 12.6 shoots per explants and a mean shoot length of 8 mm were obtained after multiplication stage. Shoot induction appeared to be strongly influenced by genotype and explant type. The percentage of shoot induction from cotyledon proximal parts ranged from 23.3% to 64.0% according to the genotype. Efficient rooting was achieved on half-solid MS medium containing 0.1 mg/l 1-Naphthaleneactic acid or without growth regulator. Acclimatised plantlets were transferred to greenhouse where they grew and flowered like seeded plantlets. [less ▲]

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See detailDetermination of absolute molecular weight of bioactive polycations
Plotnikova, Evgeniya ULg; Sevrin, Chantal ULg; Claes, Nicolas et al

Poster (2015)

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See detailDetermination of Absolute Strengths of N2 Quadrupole Lines From High-Resolution Ground-based IR Solar Observations
Demoulin, Philippe ULg; Farmer, C.B.; Rinsland, C.P. et al

in Journal of Geophysical Research (1991), 96(D7), 13003-13008

High-resolution, high signal-to-noise ratio, solar absorption spectra recorded with a Fourier transform spectrometer at the International Scientific Station of the Jungfraujoch, Switzerland, have been ... [more ▼]

High-resolution, high signal-to-noise ratio, solar absorption spectra recorded with a Fourier transform spectrometer at the International Scientific Station of the Jungfraujoch, Switzerland, have been analyzed to determine the strengths of several lines belonging to the S branch of the N2 (1-0) electric quadrupole vibration-rotation band centered at 2329.9168 cm-1. The method which was applied here was based on equivalent width measurements of lines observed over a broad range of air masses; extrapolation of these measurements to zero air mass gave the line strengths for the transitions S7 to S10, independent of half widths, an ambiguity unavoidable with the use of curve-fitting techniques. The resulting absolute accuracies of the line strengths derived here, estimated to be better than +-2.5% for S8, +-2.6% for S10, +-3.4% for S9, and +-5.1% for S7, are due largely to the high quality and quantity of the spectra retained in this analysis and the accuracy with which the observation conditions are known. An important application of the improved values for these N2 transitions, which have low initial ground state energies, is the direct determination of the line-of-sight atmospheric air masses associated with remotely sensed infrared spectroscopic observations. Positions of the N2 transitions studied here have further been redetermined with an absolute accuracy better than 0.0002 cm-1. [less ▲]

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See detailDetermination of acidic and basic drugs by capillary zone electrophoresis
Crommen, Jacques ULg; Bechet, I.; Fillet, Marianne ULg et al

Conference (1994)

Detailed reference viewed: 10 (1 ULg)
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See detailDetermination of activation yield curves for fusion escaping particle diagnostics
Strivay, David ULg; Bonheure, George; Delvigne, Thierry et al

Conference (2013, June)

Detailed reference viewed: 22 (7 ULg)
Peer Reviewed
See detailDetermination of activation yields for fusion plasma escaping charged particles diagnostics
Chene, Grégoire ULg; Bonheure, George; Delvigne, Thierry et al

Conference (2013, June)

Detailed reference viewed: 22 (5 ULg)
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See detailDetermination of affinity, stoichiometry and sequence selectivity of minor groove binder complexes with double-stranded oligodeoxynucleotides by electrospray ionization mass spectrometry
Rosu, Frédéric ULg; Gabelica, Valérie ULg; Houssier, Claude ULg et al

in Nucleic Acids Research (2002), 30(16), 82

Electrospray mass spectrometry was evaluated regarding the reliability of the determination of the stoichiometries and equilibrium association constants from single spectra. Complexes between minor groove ... [more ▼]

Electrospray mass spectrometry was evaluated regarding the reliability of the determination of the stoichiometries and equilibrium association constants from single spectra. Complexes between minor groove binders (Hoechst 33258, Hoechst 33342, DAPI, netropsin and berenil) and 12mer oligonucleotide duplexes with a central sequence (A/T)(4) flanked by G/C base pairs were chosen as model systems. To validate the electrospray ionization mass spectrometry (ESI-MS) method, comparisons were made with circular dichroism and fluorescence spectroscopy measurements. ESI-MS allowed the detection of minor (2 drug + DNA) species for Hoechst 33258, Hoechst 33342, DAPI and berenil with duplex d(GGGG(A/T)(4)GGGG). d(CCCC(A/T)(4)CCCC), which were undetectable with the other techniques. Assuming that the duplexes and the complexes have the same electrospray response factors, the equilbrium association constants of the 1:1 and 2:1 complexes were determined by ESI-MS, and the values show a good quantitative agreement with fluorescence determined constants for Hoechst 33258 and Hoechst 33342. It is also shown that ESI-MS can quickly give reliable information on the A/T sequence selectivity of a drug: the signal of a complex is directly related to the affinity of the drug for that particular duplex. The potential of ESI-MS as a qualitative and quantitative affinity screening method is emphasized. [less ▲]

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See detailDetermination of air‐sea ice transfer coefficient for CO2: Significant contribution of gas bubble transport during sea ice growth
Kotovitch, Marie ULg; Moreau, S.; Zhou, Jiayun et al

Poster (2015, September)

Air‐ice CO2 fluxes were measured continuously from the freezing of a young sea‐ice cover until its decay. Cooling seawater was as a sink for atmospheric CO2 but asthe ice crystalsformed,sea ice shifted to ... [more ▼]

Air‐ice CO2 fluxes were measured continuously from the freezing of a young sea‐ice cover until its decay. Cooling seawater was as a sink for atmospheric CO2 but asthe ice crystalsformed,sea ice shifted to a source releasing CO2 to the atmosphere throughout the whole ice growth. Atmospheric warming initiated the decay, re‐shifting sea‐ice to a CO2 sink. Combining these CO2 fluxes with the partial pressure of CO2 within sea ice, we determined gas transfer coefficients for CO2 at air‐ice interface for growth and decay. We hypothesize that this difference originates from the transport of gas bubbles during ice growth, while only diffusion occurs during ice melt. In parallel, we used a 1D biogeochemical model to mimic the observed CO2 fluxes. The formation of gas bubbles was crucial to reproduce fluxes during ice growth where gas bubbles may account for up to 92 % of the upward CO2 fluxes. [less ▲]

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See detailDetermination of Albendazole and Its Main Metabolites in Ovine Plasma by Liquid Chromatography with Dialysis as an Integrated Sample Preparation Technique
Chiap, Patrice ULg; Evrard, Brigitte ULg; Bimazubute, M. A. et al

in Journal of Chromatography. A (2000), 870(1-2), 121-34

Albendazole is a benzimidazole derivative with a broad-spectrum activity against human and animal helminth parasites. In order to determine the main pharmacokinetic parameters in sheep after oral and ... [more ▼]

Albendazole is a benzimidazole derivative with a broad-spectrum activity against human and animal helminth parasites. In order to determine the main pharmacokinetic parameters in sheep after oral and intravenous administration of a new formulation of albendazole (an aqueous solution), a fully automated method was developed for the determination of this drug and its main metabolites, albendazole sulfoxide (active metabolite) and sulfone in ovine plasma. This method involves dialysis as purification step, followed by enrichment of the dialysate on a precolumn and liquid chromatography (LC). All sample handling operations were executed automatically by means of an ASTED XL system. After conditioning of the trace enrichment column (TEC) packed with octadecyl silica with pH 6.0 phosphate buffer containing sodium azide, the plasma sample, in which a protein releasing reagent (1 M HCl) containing Triton X-100 was automatically added, was loaded in the donor channel and dialysed on a cellulose acetate membrane in the static-pulsed mode. The dialysis liquid consisted of pH 2.5 phosphate buffer. By rotation of a switching valve, the analytes were eluted from the TEC in the back-flush mode by the LC mobile phase and transferred to the analytical column, packed with octyl silica. The chromatographic separation was performed at 35 degrees C and the analytes were monitored photometrically at 295 nm. Due to the differences in hydrophobic character between albendazole and its metabolites, a gradient elution was applied. The mobile phase consisted of a mixture of acetonitrile and pH 6.0 phosphate buffer. The proportion of organic modifier was increased from 10.0 to 50.1% in 12.30 min, then from 50.1 to 66.9% in 1.70 min. First, the gradient conditions and the temperature were optimised for the LC separation using the DryLab software. Then, the influence of some parameters of the dialysis process on analyte recovery was investigated. Finally, the method developed was validated. The mean recoveries for albendazole and its metabolites were about 70 and 65%, respectively. The limits of quantification for albendazole and its metabolites were 10 and 7.5 ng/ml, respectively. [less ▲]

Detailed reference viewed: 40 (0 ULg)