Convective drying of wastewater sludge: Introduction of shrinkage effect in mathematical modelingBennamoun, Lyes ; Crine, Michel ; Léonard, Angélique ![]() in Drying Technology (2013), 31(6), 643-654 Detailed reference viewed: 2 (0 ULg) Convective drying of gels: comparison between simulated and experimental moisture profiles obtained by X-ray microtomography; ; et al in Drying Technology (2010), 28(5), 644-650 Detailed reference viewed: 41 (10 ULg) Convective drying of wastewater sludges: Influence of air temperature, superficial velocity, and humidity on the kineticsLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Drying Technology (2005), 23(8), 1667-1679 The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux ... [more ▼] The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux period is observed, while sludge B is characterized by a long decreasing drying flux phase. A sensitivity analysis shows that temperature is the main operating parameter affecting the drying kinetics. Mass and heat transfer coefficients as well as water evaporation capacities are calculated from drying curves. Transfer coefficients are related to operating conditions through dimensionless relations. For both sludges, a linear relation is found between water evaporation capacity and the maximal measured drying flux. [less ▲] Detailed reference viewed: 60 (10 ULg) Study of convective drying of wastewater sludges - Texture follow-up by X-ray microtomography - Thesis presented on the 7th February 2003-University of Liege, BelgiumLéonard, Angélique ![]() in Drying Technology (2004), 22(1-2), 417-419 Detailed reference viewed: 31 (7 ULg) Measurement of shrinkage and cracks associated to convective drying of soft materials by X-ray microtomographyLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Drying Technology (2004), 22(7), 1695-1708 Traditionally, the measurement of shrinkage occurring during drying is performed by destructive or poorly accurate techniques such as volume displacement methods. Cracks detection and quantification are ... [more ▼] Traditionally, the measurement of shrinkage occurring during drying is performed by destructive or poorly accurate techniques such as volume displacement methods. Cracks detection and quantification are realised either by destructive techniques or sophisticated but expensive nondestructive ones (NMR imaging). X-ray microtomography in combination with image analysis provides an accurate, nondestructive and easy to use technique to determine simultaneously shrinkage and crack extent. Results reported in this article concern drying of wastewater sludges whose management will become a real challenge in the years to come. These results show a clear relation between drying kinetics and crack development. This could be related to the development of internal diffusional limitations inducing moisture gradients and mechanical stresses leading to cracks formation. [less ▲] Detailed reference viewed: 52 (12 ULg) Multiscale texture characterization of wastewater sludges dried in a convective rigLéonard, Angélique ; Blacher, Silvia ; Pirard, René et alin Drying Technology (2003), 21(8), 1507-1526 Secondary sludges from two different wastewater treatment plants are conditioned and dewatered in the same way before drying in a lab-scale convective rig at the same operating conditions. Several ... [more ▼] Secondary sludges from two different wastewater treatment plants are conditioned and dewatered in the same way before drying in a lab-scale convective rig at the same operating conditions. Several techniques are used to characterize the texture of the dried materials over a wide range of scales from nm up to mm. Texture and porosity of the dried products are studied by SEM imaging, nitrogen absorption isotherms (0.5 < d(p) < 50 nm), mercury porosimetry (7.5 nm < d(p) < 150 mum) and X-ray microtomography (spatial resolution= 41 mum). The image analysis of cross-sections reconstructed by microtomography also allows following shrinkage and textural evolution during drying. [less ▲] Detailed reference viewed: 22 (6 ULg) Use of X-ray microtomography to follow the convective heat drying of wastewater sludgesLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Drying Technology (2002), 20(4-5), 1053-1069 X-ray microtomography is proposed as a new tool to investigate the evolution of size, shape and texture of soft materials during a drying operation. This study is focused on the drying of mechanically ... [more ▼] X-ray microtomography is proposed as a new tool to investigate the evolution of size, shape and texture of soft materials during a drying operation. This study is focused on the drying of mechanically dewatered sludges from a secondary wastewater treatment. The shrinkage phenomenon is shown to play a crucial role in the control of the drying process. The shrinkage curves are determined by analysing the shape and size of cross sectional microtomographic images of sludge extrudates at different levels of drying. The observation of drying and shrinkage curves allows us to determine 3 critical water content values, which define different drying zones where extragranular, intragranular or mixed limitations prevail. When drying is externally controlled. the decrease of the drying rate observed during experiments can be related to the reduction of the external area of the sample, i.e., to shrinkage. When drying is internally controlled, resistances inside the solid govern the process. Between these two extreme situations, the drying rate reduction is the result of both the external area decrease and the development of internal resistances limiting drying. A multizone model is proposed to describe quantitatively these observations. The analysis of the internal texture of the Sludge extrudates reveal, crack formation at the end of the drying process. The onset of crack formation is clearly related to the appearance of internal transfer limitations. i.e., humidity and temperature gradients inside the material. [less ▲] Detailed reference viewed: 50 (20 ULg) A STUDY OF VACUUM FREEZE-DRYING OF FROZEN WET PAPERSCarapelle, Alain ; ; Rabecki, Frédéric ![]() in Drying Technology (2001), 19(6), 1113-1124 Vacuum freeze-drying of frozen wet papers was investigated experimentally. A freeze-drying facility was built to study the process by monitoring the various physical parameters (pressure, sample ... [more ▼] Vacuum freeze-drying of frozen wet papers was investigated experimentally. A freeze-drying facility was built to study the process by monitoring the various physical parameters (pressure, sample temperature, heater temperature, water content of the sample and cold panel temperature). A simple phenomenological model was developed to explain experimental results. The values of the physical parameters were optimized to make the process cost effective. [less ▲] Detailed reference viewed: 42 (9 ULg) |
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