References of "Calvo Del Castillo, Helena"
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See detailPIXE Analysis for the pigment identification in the Nizet manucript (18th century)
Machowski, Mélanie ULg; Calvo Del Castillo, Helena ULg; Oger, Cécile ULg et al

Poster (2013, September)

Written in 1740, the Nizet Manuscript is a heraldry book compiling the genealogy of the Nizet family (Verviers, Belgium). It presents a large number of hand-painted heraldries in traditional heraldic ... [more ▼]

Written in 1740, the Nizet Manuscript is a heraldry book compiling the genealogy of the Nizet family (Verviers, Belgium). It presents a large number of hand-painted heraldries in traditional heraldic colours; the gold- and silver-like colours have undergone alteration and induced the degradation of the paper. The first inspection of the book with a binocular lens and UV-visible spectroscopy has led to the selection of representative points to be studied by PIXE analysis for the different groups of pigments. The PIXE measurements have been conducted with the cyclotron of the Institute of Nuclear and Atomic Physics and of Spectrometry of the University of Liege. Some pigments have been clearly identified, such as vermillion, umber or brass, while the presence of some others needs to be confirmed, for example azurite or lapis-lazuli. In the case of the green pigments and the organic ones (red, pink and black colours), the PIXE results must be completed by a molecular analysis. In order to exactly identify all the pigments, Raman analyses will be done to complete the pigment identification of the Nizet Manuscript. [less ▲]

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See detailAutomatic X-ray fluorescence scanning mobile system for 2D chemical analysis
Strivay, David ULg; Hocquet, François-Philippe; Dister, Hervé et al

Conference (2012, December)

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See detailX-ray methods
Calvo Del Castillo, Helena ULg; Strivay, David ULg

in Edwards, H; Vandenabeele, P (Eds.) Analytical Archaeometry: Selected Topics (2012)

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See detailNon-destructive characterization of the Nizet Manuscript (XVIIIth century) : first results
Machowski, Mélanie ULg; Calvo Del Castillo, Helena ULg; Hocquet, François-Philippe et al

Poster (2012, June)

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See detailElemental 2D imaging of paintings with a mobile EDXRF system
Hocquet, François-Philippe ULg; Calvo Del Castillo, Helena ULg; Cervera Xicotencatl, Ariadna ULg et al

in Analytical and Bioanalytical Chemistry (2011), 399(9), 3109-3116

Imaging techniques are now used commonly and intensively in cultural heritage object analysis. Nowadays, many different techniques in nature as well as many applications exist, where they can be applied ... [more ▼]

Imaging techniques are now used commonly and intensively in cultural heritage object analysis. Nowadays, many different techniques in nature as well as many applications exist, where they can be applied. X-ray radiography and infrared reflectography as well as UV photography are some of the most applied techniques. The study of works of art usually requires these techniques to be non-invasive. Furthermore, they are frequently required to perform in situ analysis. A few years ago, our laboratory developed a mobile energy-dispersive X-ray fluorescence and UV-vis-NIR coupled spectrometer, especially designed for fieldwork studies, where all three techniques can be applied strictly at the same site of analysis. Recent developments on a new positioning system have now allowed us to perform 2D elemental mappings with our equipment, which is especially well adapted to painting analysis. The system control is carried out entirely through a laptop computer running a dedicated homemade software. The positioning is achieved by means of a CCD camera embedded in the system and controlled via a Wi-Fi connection through the computer. The data acquisition system, which is made through a homemade multichannel pulse height analyzer, being also managed via the software mentioned above, goes through an Ethernet connection. We will present here the new developments of the system and an example of in situ 2D elemental mapping applied on an anonymous oil painting on wood panel. The discovery of a hidden painting under this oil painting makes it a good choice for a first example of 2D large scan with a mobile instrument. © Springer-Verlag 2010. [less ▲]

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See detailImaging techniques
Calvo Del Castillo, Helena ULg; Cervera Xicotencatl, Ariadna; Oger, Cécile

Conference (2010)

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See detailCombined PIXE/PIGE and IBIL with external beam applied to the analysis of Merovingian glass beads
Mathis, François ULg; Othmane, G.; Vrielynck, Olivier et al

in Nuclear Instruments & Methods in Physics Research. Section B, Beam Interactions with Materials and Atoms (2010), 268(11-12), 2078-2082

New improvements on our archaeometry line at the cyclotron of the Institute of Nuclear and Atomic Physics and of Spectrometry of the University of Liege have allowed the use of PIXE/PIGE and IBIL in-air ... [more ▼]

New improvements on our archaeometry line at the cyclotron of the Institute of Nuclear and Atomic Physics and of Spectrometry of the University of Liege have allowed the use of PIXE/PIGE and IBIL in-air for the analysis of cultural heritage objects. The extraction is performed through a 100 nm thick Si3N4 window. The detection set-up consists now of two X-ray and one gamma-ray detectors, together with a fiber optic UV-visible spectrometer. This set-up has already been tested for the analysis of modern corundum [1] and is now adapted to the analysis of archaeological artefacts. In this work, we have used it to analyse 216 out of the 5000 Merovingian glass beads that come from the necropolis of Bossut-Gottechain (Belgium), one of the most important ever found in Belgium. The IBA analyses confirmed the typological division of different beads groups through chemical composition that gives us new insights on fabrication techniques of glass matrices and colorants. (C) 2010 Elsevier B.V. All rights reserved. [less ▲]

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