References of "Douny, Caroline"
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See detailEffect of fuel and kiln type on the polycyclic aromatic hydrocarbon (PAH) levels in smoked shrimp, a Beninese food condiment
Kpoclou, Euloge; Anihouvi, Victor; Azokpota, Paulin et al

in Food Additives & Contaminants. Part A. Chemistry, Analysis, Control, Exposure & Risk Assessment (2014), 31(7), 1212-1218

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See detailEffect of fuel and kiln type on the polycyclic aromatic hydrocarbon (PAH) levels in smoked shrimp, a Beninese food condiment
Kpoclou, Euloge; Anihouvi, Victor; Azokpota, Paulin et al

in Food Additives & Contaminants. Part A. Chemistry, Analysis, Control, Exposure & Risk Assessment (2014), 31(7), 1212-1218

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See detailEffect of fuel and kiln type on the polycyclic aromatic hydrocarbon (PAH) levels in smoked shrimp, a Beninese food condiment
Kpoclou, Euloge; Anihouvi, Victor; Azokpota, Paulin et al

in Food Additives & Contaminants. Part A. Chemistry, Analysis, Control, Exposure & Risk Assessment (2014), 31(7), 1212-1218

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See detailMicrobial, biochemical and sensorial quality assessment of Algerian farmed tilapia (Oreochromis niloticus) stored at 4 and 30°C
Dergal, Nadir; Abi-Ayad, S.M.E.-A.; Degand, Guy ULg et al

in African Journal of Food Science (2013), 7(12), 498-507

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See detailValidation of a LC-MS analytical method for the measurement of aldehydes in meat and oil
Tihon, Angélique; Douny, Caroline ULg; Bayonnet, Pierre ULg et al

Poster (2013, April 18)

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See detailDevelopment of an analytical method to detect metabolites of nitrofurans. Application to the study of furazolidone elimination in Vietnamese black tiger shrimp (Penaeus monodon)
Douny, Caroline ULg; Widart, Joëlle ULg; De Pauw, Edwin ULg et al

in Aquaculture (2013), 376-379

Nitrofurans, banned antibiotics in European Union (EU), have often been found in imported aquaculture products in the past and are still found nowadays according to the Rapid Alert System for Feed and ... [more ▼]

Nitrofurans, banned antibiotics in European Union (EU), have often been found in imported aquaculture products in the past and are still found nowadays according to the Rapid Alert System for Feed and Food (RASFF) of the European Commission. A quantitative method based on liquid chromatography coupled to isotopic dilution tandem mass spectrometry (LC–IDMS/MS) was developed for the determination of the residues of four nitrofuran antibiotic residues in shrimps. The experimental protocol consisted of an acid-catalysed release of protein-bound metabolites, followed by derivatisation with 2-nitrobenzaldehyde (NBA). Then, a double liquid–liquid extraction with ethyl acetate was performed before LC–IDMS/MS analysis by positive electrospray ionisation (ES+) with multiple reaction monitoring (MRM) of two transitions per compound. An “in-house” validation of the method for shrimp analysis was conducted according to the EU criteria for the analysis of veterinary drug residues in foods. The decision limits (CCalpha) were 0.08–0.36 µg kg -1 and the detection capabilities (CCbeta) were 0.12–0.61 µg kg-1, which are both below the minimum required performance limit (MRPL) set at 1 µg kg -1 by the EU. The developed method was applied to evaluate the elimination of furazolidone residues in shrimp muscles after a contamination experiment. After 28 days of decontamination, a concentration of 115 µg kg-1 of furazolidone metabolite 3-amino-2-oxazolidinone (AOZ) was still measured in shrimp muscle. [less ▲]

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See detailMicrobiological and Physico-Chemical Quality of Smoked Shrimp, An Expanding Food Condiment in Beninese Local Markets
Kpoclou, Euloge Y.; Anihouvi, Victor B.; Azokpota, Paulin et al

in Food and Public Health (2013), 3(6), 277-283

Entire Smoked Shrimp (ESS) and Smoked Shrimp Powder (SSP) are two food condiments widely used in Beninese local cooking practices. Twelve samples of each product collected from local markets were ... [more ▼]

Entire Smoked Shrimp (ESS) and Smoked Shrimp Powder (SSP) are two food condiments widely used in Beninese local cooking practices. Twelve samples of each product collected from local markets were evaluated for safety assessment using standard methods. Regarding the microbiological status of the samples, the Enterobacteriaceae were detected in 83% and 75% of ESS and SSP respectively, whereas 25% of samples of each product were found to contain E. coli. Pathogenic bacteria such as S. aureus and Salmonella were absent. Except 8% and 17% of SSP sample exceeding the maximal limit of 106 UFC/g for Aerobic Mesophilic Bacteria and 104 UFC/g Enterobacteriaceae respectively, all the other samples were within the acceptable limits. Water activity values were low, ranging between 0.54±0.01 for SSP and 0.61±0.01 for ESS, showing a potential microbial stability. Considering the chemical hazards, 15 EU priority polycyclic aromatic hydrocarbon (PAHs) were detected in the samples examined with median Benzo(a) pyrene and PAH4 contents (91 μg kg-1 and 490 μg kg-1respectively) exceeding the European maximal limit (5.0 μg kg-1 and 30 μg kg-1). This study showed that smoked shrimps may be generally safe from a microbiological point of view, but they constitute a large source of exposure to possible carcinogenic PAHs. [less ▲]

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See detailDetermination of chloramphenicol in honey, shrimp and poultry meat with liquid chromatography-mass spectrometry. Validation of the method according to Commission Decision 2002/657/EC
Douny, Caroline ULg; Widart, Joëlle ULg; De Pauw, Edwin ULg et al

in Food Analytical Methods (2013), 6(5), 1458-1465

Chloramphenicol (CAP) is an antibiotic used for the treatment of bacterial infections in human and veterinary medicine. The use of CAP was prohibited in the European Union in 1994. Control laboratories ... [more ▼]

Chloramphenicol (CAP) is an antibiotic used for the treatment of bacterial infections in human and veterinary medicine. The use of CAP was prohibited in the European Union in 1994. Control laboratories are required to use suitably validated analytical methods to check sample compliance with the regulation. A quantitative method based on liquid chromatography coupled to isotopic dilution tandem mass spectrometry (LC–IDMS/MS) was developed for the determination of chloramphenicol in honey, shrimp and poultry meat. The experimental protocol consisted of a liquid-liquid extraction with ethyl acetate. Separation and detection were realized respectively by a 2690 Waters HPLC (Milford, MA, USA) and a Micromass Triple Quadrupole mass spectrometer (Micromass, Manchester, UK), equipped with an Electrospray source. The effects of mobile phase additives on the response of LC/ESI/MS were examined. Two different HPLC columns were tested: the X-Terra from Waters and the Alltima HP C18 HL from Alltech (Deerfield, IL, USA). A validation of the method was conducted according to the EU criteria for the analysis of chloramphenicol in foods. The decision limits (CCα) were 0.04, 0.03, 0.07 µg kg-1 and the detection capabilities (CCβ) were 0.05, 0.04, 0.08 µg kg-1 for honey, shrimp and poultry meat respectively. Those values are below the minimum required performance limit (MRPL) set at 0.3 µg kg-1 by the EU and 0.1 µg kg-1 by Belgium. Our protocol has the advantage to propose a unique extraction method working as well for honey, shrimp and poultry meat, contrary to similar published methods in which a different extraction method is used for each type of matrix. [less ▲]

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See detailPreliminary Evaluation of Antimicrobial Residue Levels in Marketed Pork and Chicken Meat in the Red River Delta Region of Vietnam
pham kim, Dang; Degand, Guy ULg; Douny, Caroline ULg et al

in Food and Public Health (2013), 3(6), 267-276

The presence of antibacterial in 97 pork and 83 chicken meat samples, randomly collected from 3 different representative provinces (Hanoi, Hai Duong and Thai Binh) of the Red River Delta, was determined ... [more ▼]

The presence of antibacterial in 97 pork and 83 chicken meat samples, randomly collected from 3 different representative provinces (Hanoi, Hai Duong and Thai Binh) of the Red River Delta, was determined by a screening step using in parallel 2 microbiological methods (Premi®-test and New Two Plate Test). In total, 27% of all samples displayed a positive response in at least one of both tests, from which 11 (13% of chicken samples) are chicken samples and 38 (39% of pork samples) are pork samples. The 33 samples from the Thai Binh which were screened positive were then submitted to post-screening tests specific for tetracyclines and (fluoro) quinolones (Tetrasensor® dipstick for tetracyclines and an ELISA for quinolones), two groups of antibiotics widely used in animal production in this region, and confirmed by liquid chromatography coupled to mass spectrometry. Tetracyclines and (fluoro)quinolones residues were found, using a post screening test, in 23 and 5 samples, respectively. Ten (all pork) and 4 samples (1 pork, 3 chicken) were confirmed containing tetracyclines (chlortetracycline, oxytetracycline, tetracycline, doxycycline) and (fluoro) quinolones (nalidixic acid, enrofloxacin and ciprofloxacin) respectively, from which 1 and 3 pork samples were found to contain enrofloxacin and tetracycline residues , respectively, with a concentration higher than their respective MRLs. This study shows the good performance of the proposed strategy to identify non-compliant meat samples (microbiological screening, tetracyclines and quinolones targeted post-screening and confirmation), which allows to obtain conclusive results in 82% of the cases. [less ▲]

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See detailFirst Survey on the Use of Antibiotics in Pig and Poultry Production in the Red River Delta Region of Vietnam
Pham Kim, Dang; Saegerman, Claude ULg; Douny, Caroline ULg et al

in Food and Public Health (2013), 3(5), 247-256

In Vietnam where epidemics occur regularly in animal production, the farmers consider antibiotics as one of the solutions to fight against livestock diseases, thus the risk of abuse, even illegal use of ... [more ▼]

In Vietnam where epidemics occur regularly in animal production, the farmers consider antibiotics as one of the solutions to fight against livestock diseases, thus the risk of abuse, even illegal use of antibiotics in livestock is very high. However, this is a recent issue and has not yet been thoroughly investigated. A cross-sectional study on the use of antibiotics in pig and poultry production as well as the farmer’s knowledge on the danger of the antibiotic use in three different animal production systems (farm household, semi-industrial and industrial) was conducted from July 2009 to March 2010 on 270 entities, in 3 representative localities of the Red River Delta (RRD). The results showed that a large volume of antibiotics was used arbitrary in all animal production systems. Animals were not only treated for acute diseases, but also for disease prevention, and for growth promotion. At least 45 antibiotics of more than 10 classes were used. Fifteen antibiotics were used in pig and poultry feed. For diseases treatment and prevention, antibiotics were used abusively and even illegally (e.g. chloramphenicol) by both farmers and veterinarians. The findings of this survey will permit developing new strategies for prudent use of antibiotics in livestock in Vietnam. These results will help not only to strengthen issues such as veterinary networks; antibiotics use guidance, residues monitoring systems and food safety, but also to improve awareness and ethics of producers and veterinary drug sellers. [less ▲]

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See detailFirst evidence of the possible implication of the 11-deoxycorticosterone (DOC) in immune activity of Eurasian perch (Perca fluviatilis, L.): Comparison with cortisol
Mathieu, Cédric; Mila, Sylvain; Mandiki, Robert et al

in Comparative Biochemistry & Physiology Part A : Molecular & Integrative Physiology (2013), 165(2), 149-158

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See detailQuantification of Acrylamide in Various Belgian Potato Products Using Solid Phase Extraction and Liquid Chromatography Tandem Mass Spectrometry Detection
Douny, Caroline ULg; Widart, Joëlle ULg; Maghuin-Rogister, Guy ULg et al

in Food and Public Health (2012), 2(5), 137-141

Acrylamide (CH2=CHCONH2), a neurotoxic and potentially carcinogenic substance for human health, is in the glare of the spotlights for a few years. This is mostly due to the fact that acrylamide was found ... [more ▼]

Acrylamide (CH2=CHCONH2), a neurotoxic and potentially carcinogenic substance for human health, is in the glare of the spotlights for a few years. This is mostly due to the fact that acrylamide was found worldwide in various heated foodstuffs. Levels reported in the literature vary from 25 to 2000 ìg/kg and potato products are considered as the most contaminated. A possible pathway of synthesis of acrylamide is the Maillard reaction between reducing sugars and the amino acid asparagine. The aim of this study was to develop a liquid chromatography/mass spectrometry method to analyse as quickly as possible acrylamide in a variety of Belgian food samples such as potatoes, French fries, crisp bread, coffee, corn-flakes, etc. The sample preparation consisted in a liquid/liquid extraction, a centrifugation, followed by purification with Solid Phase Extraction (SPE). The instruments used were a Waters 2690 Alliance HPLC system coupled to a Micro-mass Quattro Ultima Platinum triple-quadrupole mass spectrometer. The analysis was performed in MS/MS mode using isotopic dilution technique for quantification. An internal 13C3 labelled standard was added prior to extraction. Quantifica-tion in MS/MS mode was calculated by reconstructing the ion current with the most abundant daughter ions for native and 13C labelled standard (ions of m/z 55 and 58). [less ▲]

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See detailScreening, post-screening and confirmation analysis of antibiotics in pork and chicken meat marketed in Vietnam.
Pham Kim, Dang; Degand, Guy ULg; Douny, Caroline ULg et al

in EuroResidue VII: conference on residues of veterinary drugs in food (2012)

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See detailAnalyse sensorielle et biochimique du Tilapia du Nil (Oreochromis niloticus) conservé à température ambiante (30°C) et à 4°C
Boudjlal Dergal, Nadir; Ali-Mehidi, Smaïl; Douny, Caroline ULg et al

Poster (2012)

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See detailFood interactions : effects on health, consumer perception and impact on agro-food industries “FOODINTER”.
Scippo, Marie-Louise ULg; Blust, Ronny; Boniver, Delphine et al

Report (2011)

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See detailDevelopment of a LC-UV-MS analytical method for malondialdehyde.
Douny, Caroline ULg; Dure, Remy; Brose, François ULg et al

Poster (2011)

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