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See detailDyBa2Cu307-Y superconducting materials synthesized in-situ in a magnetic-field - relations between structure and properties
Cloots, Rudi ULg; Diko, P.; Godelaine, P. A. et al

in Physica C: Superconductivity (1994), 235(Part 1), 357-358

We have synthesized c-axis oriented magnetically melt textured grown DyBa2Cu3O7-y samples at 1035 degrees C under 0.6 T magnetic induction. We discuss the crystal growth mechanism of such 123 melt ... [more ▼]

We have synthesized c-axis oriented magnetically melt textured grown DyBa2Cu3O7-y samples at 1035 degrees C under 0.6 T magnetic induction. We discuss the crystal growth mechanism of such 123 melt textured grown superconducting ceramics. A strictly tridimensional model is proposed based on Schmitz et al. model, taking into account the peculiar physical properties reported for such materials. In particular a filamentary one dimensional electron conduction path at the percolation threshold is emphasized. We have used optically polarized ligth microscopy as well as electron microscopy analysis to deduce the growth steps. [less ▲]

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See detailSTUDY OF THE CRYSTALLIZATION PROCESS IN BI2-XPBXSR2CA2CU3O10-Y GLASS SYSTEMS - OPTICAL POLARIZED-LIGHT MICROSCOPY, ELECTRICAL AND MAGNETIC-PROPERTIES
Cloots, Rudi ULg; Romain, Anne-Claude ULg; Rulmont, André ULg et al

in Superconductor Science & Technology (1993), 6(12), 850-857

Synthesis of Bi2-xPbxSr2Ca2Cu3O10-y (x = 0 and x = 0.3) has been performed using the glass recrystallization route technique. After splat quenching, the samples were annealed at 820, 850 or 870-degrees-C ... [more ▼]

Synthesis of Bi2-xPbxSr2Ca2Cu3O10-y (x = 0 and x = 0.3) has been performed using the glass recrystallization route technique. After splat quenching, the samples were annealed at 820, 850 or 870-degrees-C for 96 or 144 h (with one intermediary grinding). High-resolution polarization micrographs and electrical (and magnetic susceptibility) measurements have been taken. Various growth mechanisms can thus be checked, and the physical properties are studied in relation to the microstructure. It is found that the 2223 phase does not crystallize directly from the amorphous one but results from a dissolution-reprecipitation process. The stability of the 2212 phase is emphasized. The 2201 phase precipitates at high temperature and rapidly reacts with the melt to form the 2223 phase. The kinetics of the lead-substituted sample seems to be controlled by the Ca2PbO4 phase. which acts as a flux. [less ▲]

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