Gas-liquid mass transfer in a circulating jet-loop nitrifying MBR; Salmon, Thierry ; Toye, Dominique et alin Chemical Engineering Science (2005), 60(22 Sp. Iss. SI), 6346-6353 Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water ... [more ▼] Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water forced circulation are adopted to obtain a high biomass retention time and to achieve a separate control of mixing and aeration. This study is intended to determine how gas-liquid mass transfer is affected by operating conditions. In a first approximation, liquid was assumed to be perfectly mixed. A classical non-steady state clean water test, known as the "gas out-gas in" method, was used to determine the gas-liquid mass transfer coefficient k(L)a. Air and recirculated liquid superficial velocities were gradually increased from 0.013 to 0.019m s(-1) and 0.0056 to 0.011 m s(-1), respectively. Subsequently, the gas-liquid mass transfer coefficient kLa varied from 0.01 to 0.02 s(-1). It appears to be influenced by the combined action of air and recirculated liquid flowrates in the range 0.72-1.03N m(3) h(-1) and 0.30-0.58 m(3) h(-1), respectively, for air and liquid. Correlations are proposed to describe this double influence. Experiments were performed on tap water and a culture medium used for the autotrophic growth of nitrifying bacteria, respectively. Oxygen transfer appeared to be not significantly affected by the mineral salt (0.48 g 1(-1)) encountered in this medium. (c) 2005 Elsevier Ltd. All rights reserved. [less ▲] Detailed reference viewed: 58 (5 ULg) Analysis of gas holdup in bubble columns with non-Newtonian fluid using electrical resistance tomography and dynamic gas disengagement technique; ; Marchot, Pierre et alin Chemical Engineering Science (2005), 60(22 Sp. Iss. SI), 6118-6123 This paper presents an experimental analysis of the influence of the liquid rheology on the gas flow pattern in a bubble column reactor. Aqueous solutions of xanthan are selected as an example of non ... [more ▼] This paper presents an experimental analysis of the influence of the liquid rheology on the gas flow pattern in a bubble column reactor. Aqueous solutions of xanthan are selected as an example of non-Newtonian shear thinning fluid. Averaged gas holdup is determined by two experimental techniques: parietal pressure probes and electrical resistance tomography (ERT). ERT is also used to provide 2D images of the gas phase distribution in a column cross-section. Bubble size distributions are evaluated by a gas disengagement technique using the parietal pressure probes. All these techniques clearly show the gas flow pattern is different in Newtonian and non-Newtonian fluids. Gas holdup values decrease when increasing the liquid viscosity and reach a minimum or a plateau. Homogeneous flow regime, observed in water at low gas velocities, tends to disappear when viscosity increases. This evolution is visualized by a much less isotropic distribution of the gas phase within cross-section of the column and by the appearance of much larger bubbles due to an increased coalescence phenomenon. (c) 2005 Elsevier Ltd. All rights reserved. [less ▲] Detailed reference viewed: 39 (0 ULg) Imaging of liquid distribution in reactive distillation packings with a new high-energy x-ray tomographToye, Dominique ; Crine, Michel ; Marchot, Pierre ![]() in Measurement Science & Technology (2005), 16(11), 2213-2220 We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and ... [more ▼] We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and reactive distillation columns. The first results obtained with this set-up on test objects (physical phantoms), such as a cylindrical container filled with water or a large diameter structured metallic packing, validate the technique as a quantitative tool for geometrical measurements. Very detailed two-dimensional (21)) and three-dimensional (3D) images of a 0.09 m diameter KATAPAK-SP 12, a reactive distillation packing, are presented. Quantitative information relative to liquid hold-up distribution may be obtained from tomographic imaging performed on an irrigated column packed with this element. [less ▲] Detailed reference viewed: 35 (6 ULg) Analyse quantitative de la texture poreuse d'un matériau polymère cellulaire basée sur des images de microtomographie à rayons X; Toye, Dominique ; et alPoster (2005, October) Detailed reference viewed: 15 (0 ULg) Étude de la texture poreuse d'un matériau polymère cellulaire utilisé en ingénierie tissulaire par microtomographie à rayons X; Toye, Dominique ; et alPoster (2005, October) Detailed reference viewed: 33 (6 ULg) Mass transfer, mixing and gas hold-up in a circulating jet-loop nitrifying MBR; Salmon, Thierry ; Toye, Dominique et alin Proceedings of 7th World Congress of Chemical Enginnering - WCCE7, Glasgow, Scotland, 10-14 July 2005 (2005) Detailed reference viewed: 15 (1 ULg) Integrated adsorbent and process characterization. Application to air separation PSA processes; ; et al Conference (2005) Detailed reference viewed: 14 (2 ULg) Utilisation d’un nouveau tomographe à haute énergie pour extraire l’information structurale d’un échantillon de dévésiculeur; Toye, Dominique ; Marchot, Pierre et alPoster (2005) Detailed reference viewed: 9 (0 ULg) High energy, high resolution x-ray tomography applied to catalytic distillation packingsToye, Dominique ; ; Marchot, Pierre et alConference (2005) Detailed reference viewed: 8 (1 ULg) Transfert de matière gaz-liquide et mélange dans un réacteur membranaire à recirculation interne; Salmon, Thierry ; et alin Azzaro-Pantel, C.; Bertrand, J.; Cabassud, M. (Eds.) et al Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 81 (1 ULg) 3D imaging of reactive distillation packings with a new high energy x-ray tomographToye, Dominique ; ; Crine, Michel et alin Jong, A.; Takei, M.; William, R. A. (Eds.) et al Proceedings of 4th World Congress in Industrial Process Tomography (WCIPT4), Aizu, Japan, 5-8 septembre 2005 (2005) Detailed reference viewed: 24 (4 ULg) Evolution de l'écoulement de fluides non-newtoniens avec le temps d'agitation en cuve agitée par vélocimétrie par images de particules; Marchot, Pierre ; Toye, Dominique et alin SFGP (Ed.) Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 8 (4 ULg) Possibilities and limits of application of electrical resistance tomography in hydrodynamics of bubble columnsToye, Dominique ; ; Simon, Daniel et alin Canadian Journal of Chemical Engineering (2005), 83(1), 4-10 Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the ... [more ▼] Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the potentialities of an Electrical Resistance Tomography (ERT) device. We analyse cross correlation of electrode pair measurements, of neighbouring pixels and power spectra of averaged pixels within a single plane as well as cross correlations of averaged pixels between two planes, without finding a clear signature of the churn turbulent flow. Variable gas flow rate inputs are used to determine the time resolution of the ERT. [less ▲] Detailed reference viewed: 32 (14 ULg) Image reconstruction in X-ray tomographyToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 13 (5 ULg) Computed Tomography at the University of Liège – Chemical Engineering LaboratoryToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 9 (1 ULg) Computed X-ray tomography investigations in packed bedsToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 12 (3 ULg) Electrical tomography investigation in bubble columnsToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 10 (2 ULg) Visualisation de l'écoulement d'un fluide Non-Newtonien en cuve agitée par Vélocimétrie par Images de Particules : influence du temps de mélange; Marchot, Pierre ; Toye, Dominique et alPoster (2004) Detailed reference viewed: 23 (1 ULg) Flow visualisation of non-Newtonian fluids in a stirred tank using Particle Image Velocimetry : evolution with time; Marchot, Pierre ; Toye, Dominique et alConference (2004) Detailed reference viewed: 7 (0 ULg) Flow Pattern Evolution With Time Mixing Of Non-Newtonian Fluid In A Stirred Tank Using Particle Image Velocimetry; Marchot, Pierre ; Toye, Dominique et alin American Society of Mechanical Engineering (ASME) (Ed.) Proccedings of 7th Biennal ASME Conference, Engineering Systems Design and Analysis – ESDA 2004, Manchester, United Kingdom,19 – 22 July 2004 (2004) Detailed reference viewed: 10 (0 ULg) |
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