Caractérisation des écoulements en présence d’un agitateur rotor-stator et d’un fluide non newtonien en cuve agitée par vélocimétrie par images de particules; Marchot, Pierre ; Toye, Dominique et alPoster (2006) Detailed reference viewed: 13 (0 ULg) Etude du colmatage dans un bioréacteur membranaire à recirculation externe utilisé en nitrification partielle; Pirard, Jean-Paul ; Marchot, Pierre et alin Proceedings of MEMPRO 3 - Intégration des membranes dans les procédés (2006) Detailed reference viewed: 22 (2 ULg) Influence of operating parameters on nitrite; Salmon, Thierry ; Marchot, Pierre et alin Proceeding of the International Symposium on Environmental Biotechnology (2006) Detailed reference viewed: 19 (2 ULg) Gas-liquid mass transfer in a circulating jet-loop nitrifying MBR; Salmon, Thierry ; Toye, Dominique et alin Chemical Engineering Science (2005), 60(22 Sp. Iss. SI), 6346-6353 Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water ... [more ▼] Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water forced circulation are adopted to obtain a high biomass retention time and to achieve a separate control of mixing and aeration. This study is intended to determine how gas-liquid mass transfer is affected by operating conditions. In a first approximation, liquid was assumed to be perfectly mixed. A classical non-steady state clean water test, known as the "gas out-gas in" method, was used to determine the gas-liquid mass transfer coefficient k(L)a. Air and recirculated liquid superficial velocities were gradually increased from 0.013 to 0.019m s(-1) and 0.0056 to 0.011 m s(-1), respectively. Subsequently, the gas-liquid mass transfer coefficient kLa varied from 0.01 to 0.02 s(-1). It appears to be influenced by the combined action of air and recirculated liquid flowrates in the range 0.72-1.03N m(3) h(-1) and 0.30-0.58 m(3) h(-1), respectively, for air and liquid. Correlations are proposed to describe this double influence. Experiments were performed on tap water and a culture medium used for the autotrophic growth of nitrifying bacteria, respectively. Oxygen transfer appeared to be not significantly affected by the mineral salt (0.48 g 1(-1)) encountered in this medium. (c) 2005 Elsevier Ltd. All rights reserved. [less ▲] Detailed reference viewed: 58 (5 ULg) Analysis of gas holdup in bubble columns with non-Newtonian fluid using electrical resistance tomography and dynamic gas disengagement technique; ; Marchot, Pierre et alin Chemical Engineering Science (2005), 60(22 Sp. Iss. SI), 6118-6123 This paper presents an experimental analysis of the influence of the liquid rheology on the gas flow pattern in a bubble column reactor. Aqueous solutions of xanthan are selected as an example of non ... [more ▼] This paper presents an experimental analysis of the influence of the liquid rheology on the gas flow pattern in a bubble column reactor. Aqueous solutions of xanthan are selected as an example of non-Newtonian shear thinning fluid. Averaged gas holdup is determined by two experimental techniques: parietal pressure probes and electrical resistance tomography (ERT). ERT is also used to provide 2D images of the gas phase distribution in a column cross-section. Bubble size distributions are evaluated by a gas disengagement technique using the parietal pressure probes. All these techniques clearly show the gas flow pattern is different in Newtonian and non-Newtonian fluids. Gas holdup values decrease when increasing the liquid viscosity and reach a minimum or a plateau. Homogeneous flow regime, observed in water at low gas velocities, tends to disappear when viscosity increases. This evolution is visualized by a much less isotropic distribution of the gas phase within cross-section of the column and by the appearance of much larger bubbles due to an increased coalescence phenomenon. (c) 2005 Elsevier Ltd. All rights reserved. [less ▲] Detailed reference viewed: 39 (0 ULg) Imaging of liquid distribution in reactive distillation packings with a new high-energy x-ray tomographToye, Dominique ; Crine, Michel ; Marchot, Pierre ![]() in Measurement Science & Technology (2005), 16(11), 2213-2220 We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and ... [more ▼] We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and reactive distillation columns. The first results obtained with this set-up on test objects (physical phantoms), such as a cylindrical container filled with water or a large diameter structured metallic packing, validate the technique as a quantitative tool for geometrical measurements. Very detailed two-dimensional (21)) and three-dimensional (3D) images of a 0.09 m diameter KATAPAK-SP 12, a reactive distillation packing, are presented. Quantitative information relative to liquid hold-up distribution may be obtained from tomographic imaging performed on an irrigated column packed with this element. [less ▲] Detailed reference viewed: 35 (6 ULg) Analyse quantitative de la texture poreuse d'un matériau polymère cellulaire basée sur des images de microtomographie à rayons X; Toye, Dominique ; et alPoster (2005, October) Detailed reference viewed: 15 (0 ULg) Étude de la texture poreuse d'un matériau polymère cellulaire utilisé en ingénierie tissulaire par microtomographie à rayons X; Toye, Dominique ; et alPoster (2005, October) Detailed reference viewed: 33 (6 ULg) Image analysis of X-ray microtomograms of soft materials during convective drying: 3D measurementsLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Journal of Microscopy-Oxford (2005), 218(Pt 3), 247-252 Drying dewatered sludge leads to a complex three-dimensional porous structure. Moreover, this operation is dependent on the way the material is processed. In this study, textural changes of sludge ... [more ▼] Drying dewatered sludge leads to a complex three-dimensional porous structure. Moreover, this operation is dependent on the way the material is processed. In this study, textural changes of sludge extrudates submitted to convective drying are followed by a 3D image analysis of reconstructed X-ray microtomograms. To achieve this goal, two different wastewater sludges collected in wastewater treatment plant after the thickening step and dewatered in the laboratory are used. It is showed that the evolution of the 3D-crack ratio vs. the residual water content evolves following a hyperbolic law. The 3D opening crack size distribution reveals two different types of pore development, i.e. a continuous pore size evolution for one sludge and the sudden appearance of cracks for the other sludge. [less ▲] Detailed reference viewed: 48 (3 ULg) Moisture profiles determination during convective drying using x-ray microtomographyLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Canadian Journal of Chemical Engineering (2005), 83(1), 127-131 The knowledge of internal moisture profiles which develop during drying is essential for model validation purposes, but they are difficult to determine experimentally. This paper shows that X-ray ... [more ▼] The knowledge of internal moisture profiles which develop during drying is essential for model validation purposes, but they are difficult to determine experimentally. This paper shows that X-ray microtomography, together with image analysis, provides an accurate, non destructive and easy to use technique to determine moisture profiles. Results reported concern the drying of wastewater sludges whose management is becoming a real environmental challenge. An analysis of the development of moisture gradients at the sample external wall shows an influence of drying operating conditions. Finally, mass diffusion coefficients are estimated from the knowledge of both the moisture gradients and the drying flux. [less ▲] Detailed reference viewed: 38 (12 ULg) Mass transfer, mixing and gas hold-up in a circulating jet-loop nitrifying MBR; Salmon, Thierry ; Toye, Dominique et alin Proceedings of 7th World Congress of Chemical Enginnering - WCCE7, Glasgow, Scotland, 10-14 July 2005 (2005) Detailed reference viewed: 15 (1 ULg) Integrated adsorbent and process characterization. Application to air separation PSA processes; ; et al Conference (2005) Detailed reference viewed: 14 (2 ULg) Utilisation d’un nouveau tomographe à haute énergie pour extraire l’information structurale d’un échantillon de dévésiculeur; Toye, Dominique ; Marchot, Pierre et alPoster (2005) Detailed reference viewed: 9 (0 ULg) High energy, high resolution x-ray tomography applied to catalytic distillation packingsToye, Dominique ; ; Marchot, Pierre et alConference (2005) Detailed reference viewed: 8 (1 ULg) Transfert de matière gaz-liquide et mélange dans un réacteur membranaire à recirculation interne; Salmon, Thierry ; et alin Azzaro-Pantel, C.; Bertrand, J.; Cabassud, M. (Eds.) et al Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 81 (1 ULg) 3D imaging of reactive distillation packings with a new high energy x-ray tomographToye, Dominique ; ; Crine, Michel et alin Jong, A.; Takei, M.; William, R. A. (Eds.) et al Proceedings of 4th World Congress in Industrial Process Tomography (WCIPT4), Aizu, Japan, 5-8 septembre 2005 (2005) Detailed reference viewed: 24 (4 ULg) Evolution de l'écoulement de fluides non-newtoniens avec le temps d'agitation en cuve agitée par vélocimétrie par images de particules; Marchot, Pierre ; Toye, Dominique et alin SFGP (Ed.) Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 8 (4 ULg) Possibilities and limits of application of electrical resistance tomography in hydrodynamics of bubble columnsToye, Dominique ; ; Simon, Daniel et alin Canadian Journal of Chemical Engineering (2005), 83(1), 4-10 Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the ... [more ▼] Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the potentialities of an Electrical Resistance Tomography (ERT) device. We analyse cross correlation of electrode pair measurements, of neighbouring pixels and power spectra of averaged pixels within a single plane as well as cross correlations of averaged pixels between two planes, without finding a clear signature of the churn turbulent flow. Variable gas flow rate inputs are used to determine the time resolution of the ERT. [less ▲] Detailed reference viewed: 32 (14 ULg) Convective drying of wastewater sludges: Influence of air temperature, superficial velocity, and humidity on the kineticsLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Drying Technology (2005), 23(8), 1667-1679 The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux ... [more ▼] The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux period is observed, while sludge B is characterized by a long decreasing drying flux phase. A sensitivity analysis shows that temperature is the main operating parameter affecting the drying kinetics. Mass and heat transfer coefficients as well as water evaporation capacities are calculated from drying curves. Transfer coefficients are related to operating conditions through dimensionless relations. For both sludges, a linear relation is found between water evaporation capacity and the maximal measured drying flux. [less ▲] Detailed reference viewed: 56 (10 ULg) Wastewater sludge convective drying: Influence of sludge originLéonard, Angélique ; ; Salmon, Thierry et alin Environmental Technology (2004), 25(9), 1051-1057 This paper deals with thermal drying of wastewater sludges, whose management will become crucial in the forthcoming years. Sludges collected after mechanical dewatering in 5 different WWTPs are submitted ... [more ▼] This paper deals with thermal drying of wastewater sludges, whose management will become crucial in the forthcoming years. Sludges collected after mechanical dewatering in 5 different WWTPs are submitted to the same convective drying treatment in order to try finding some relations between the drying behaviours, the type of effluent and wastewater treatments. Results show clearly sludge drying remains a particularly complex operation because sludges may exhibit very different behaviours, both from kinetic and texture points of view. Initial moisture content and global composition are not sufficient to explain the different observed behaviours. It is too early to claim one or another type of water treatment has an influence on the drying behaviour. However, the drying rates can be classified in the inverse order of the organic content. Moreover for sludges at the same siccities, the harder the material (rheological properties), the higher the drying rate. Final textural properties can be related to the rheological properties and the internal diffusion limitations lowering the drying intensity. [less ▲] Detailed reference viewed: 72 (12 ULg) |
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