References of "Crine, Michel"
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See detailSynthesis optimization of organic xerogels produced from convective air-drying of resorcinol-formaldehyde gels
Job, Nathalie ULg; Panariello, Fabian; Marien, José ULg et al

in Journal of Non-Crystalline Solids (2006), 352(1), 24-34

Resorcinol-formaldehyde gels were produced at 50, 70 and 90 degrees C and with three different R/C ratios (500, 1000 and 2000). The effect of these variables combined with that of aging time was studied ... [more ▼]

Resorcinol-formaldehyde gels were produced at 50, 70 and 90 degrees C and with three different R/C ratios (500, 1000 and 2000). The effect of these variables combined with that of aging time was studied in order to optimize the synthesis conditions. The convective air-drying process was used, and the drying duration was studied with regard to the synthesis conditions. The aging time has no effect on the pore texture after 24 h at 90 degrees C or 48 h at 70 C, whatever the R/C value. The synthesis-aging step can be shortened by increasing the temperature. Nevertheless, the pore size tends then to decrease, especially when R/C is high, but this can be counterbalanced by increasing R/C. Moreover, bubbles often appear in the gel at high synthesis temperature, which limits the temperature to about 70 degrees C in the case of monolithic parts. At 70 degrees C and with an air velocity of 2 m/s, the elimination of 90% of the solvent requires 1 h drying when the pore size reaches 400-600 nm, 2.5 h for 50 nm wide pores and 3 h when the pore size decreases to 15-20 nm. The drying duration does not exceed 8 h in all cases and could be shortened by increasing the temperature at the end of the process. (c) 2005 Elsevier B.V. All rights reserved. [less ▲]

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See detailLiquid distribution through a Katapak column by X-ray tomography
Aferka, Saïd ULg; Saroha, Anil; Toye, Dominique ULg et al

Conference (2006)

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See detailSimple heuristic model of an aerosol filter
Lecocq, Rapahaël; Calvo, Sébastien ULg; Saroha, Anil et al

Poster (2006)

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See detailLiquid flow distribution in catalytic distillation columns : use of high-energy X-ray tomography
Aferka, Saïd ULg; Saroha, Anil; Toye, Dominique ULg et al

in AIChE (Ed.) AIChE Annual Meeting, Conference Proceedings, San Francisco, CA, United States, Nov. 12-17, 2006 (2006)

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See detailEtude du colmatage dans un bioréacteur membranaire à recirculation externe utilisé en nitrification partielle
Kouakou, Edouard; Pirard, Jean-Paul ULg; Marchot, Pierre ULg et al

in Proceedings of MEMPRO 3 - Intégration des membranes dans les procédés (2006)

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See detailInfluence of operating parameters on nitrite
Kouakou, Edouard; Salmon, Thierry ULg; Marchot, Pierre ULg et al

in Proceeding of the International Symposium on Environmental Biotechnology (2006)

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See detailMetal catalysts suppported on texture-tailored carbon xerogels
Job, Nathalie ULg; Léonard, Angélique ULg; Colomer, Jean-François et al

in Studies in Surface Science and Catalysis (2006), 162

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See detailGas-liquid mass transfer in a circulating jet-loop nitrifying MBR
Kouakou, Edouard; Salmon, Thierry ULg; Toye, Dominique ULg et al

in Chemical Engineering Science (2005), 60(22 Sp. Iss. SI), 6346-6353

Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water ... [more ▼]

Based on airlift configuration, a novel circulating jet-loop submerged membrane bioreactor (JLMBR) adapted to ammonium partial oxidation has been developed. Membrane technology and combined air and water forced circulation are adopted to obtain a high biomass retention time and to achieve a separate control of mixing and aeration. This study is intended to determine how gas-liquid mass transfer is affected by operating conditions. In a first approximation, liquid was assumed to be perfectly mixed. A classical non-steady state clean water test, known as the "gas out-gas in" method, was used to determine the gas-liquid mass transfer coefficient k(L)a. Air and recirculated liquid superficial velocities were gradually increased from 0.013 to 0.019m s(-1) and 0.0056 to 0.011 m s(-1), respectively. Subsequently, the gas-liquid mass transfer coefficient kLa varied from 0.01 to 0.02 s(-1). It appears to be influenced by the combined action of air and recirculated liquid flowrates in the range 0.72-1.03N m(3) h(-1) and 0.30-0.58 m(3) h(-1), respectively, for air and liquid. Correlations are proposed to describe this double influence. Experiments were performed on tap water and a culture medium used for the autotrophic growth of nitrifying bacteria, respectively. Oxygen transfer appeared to be not significantly affected by the mineral salt (0.48 g 1(-1)) encountered in this medium. (c) 2005 Elsevier Ltd. All rights reserved. [less ▲]

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See detailImaging of liquid distribution in reactive distillation packings with a new high-energy x-ray tomograph
Toye, Dominique ULg; Crine, Michel ULg; Marchot, Pierre ULg

in Measurement Science & Technology (2005), 16(11), 2213-2220

We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and ... [more ▼]

We describe a new, high-energy (420 kV), large-scale (0.45 m in diameter, 4 m in height) x-ray tomograph developed to investigate gas and liquid flow through fixed bed like absorption, distillation and reactive distillation columns. The first results obtained with this set-up on test objects (physical phantoms), such as a cylindrical container filled with water or a large diameter structured metallic packing, validate the technique as a quantitative tool for geometrical measurements. Very detailed two-dimensional (21)) and three-dimensional (3D) images of a 0.09 m diameter KATAPAK-SP 12, a reactive distillation packing, are presented. Quantitative information relative to liquid hold-up distribution may be obtained from tomographic imaging performed on an irrigated column packed with this element. [less ▲]

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See detailProduction de xérogels de carbone hyperporeux par séchage convectif
Léonard, Angélique ULg; Job, Nathalie ULg; Jomaa, Wahbi et al

in Azzaro-Pantel, Catherine; Bertrand, Joel; Cabassub, Michel (Eds.) et al Récents progrès en génie des procédés N° 92: 10ème Congrès de la SFGP, Toulouse 2005. Le génie des procédés vers de nouveaux espaces (2005, October)

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See detailTowards the production of carbon xerogel monoliths by optimizing convective drying conditions
Léonard, Angélique ULg; Sabatier, Françoise; Job, Nathalie ULg et al

Poster (2005, October)

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See detailAnalyse quantitative de la texture poreuse d'un matériau polymère cellulaire basée sur des images de microtomographie à rayons X
Lecocq, Raphaël; Toye, Dominique ULg; Maquet, Véronique et al

Poster (2005, October)

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See detailÉtude de la texture poreuse d'un matériau polymère cellulaire utilisé en ingénierie tissulaire par microtomographie à rayons X
Lecocq, Raphaël; Toye, Dominique ULg; Maquet, Véronique et al

Poster (2005, October)

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See detailProduction de xérogels de carbone hyperporeux par séchage convectif
Léonard, Angélique ULg; Job, Nathalie ULg; Jomaa, W. et al

Poster (2005, September 20)

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