Texture characterisation of ultramacroporous materials using x-ray microtomography: application to alumina foams and deer antlersLéonard, Angélique ; Blacher, Silvia ; et alConference (2005, September) Detailed reference viewed: 29 (3 ULg) Textural comparison of resorcinol-formaldehyde xerogels obtained by vacuum drying and convective dryingLéonard, Angélique ; Job, Nathalie ; et alPoster (2005, July 10) Detailed reference viewed: 2 (1 ULg) Textural comparison of resorcinol-formaldehyde xerogels obtained by vacuum drying and convective dryingLéonard, Angélique ; Job, Nathalie ; et alPoster (2005, July) Detailed reference viewed: 12 (1 ULg) Suitability of convective air drying for the production of porous resorcinol-formaldehyde and carbon xerogelsLéonard, Angélique ; Job, Nathalie ; Blacher, Silvia et alin Carbon (2005), 43(8), 1808-1811 Detailed reference viewed: 37 (2 ULg) Image analysis of X-ray microtomograms of soft materials during convective drying: 3D measurementsLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Journal of Microscopy-Oxford (2005), 218(Pt 3), 247-252 Drying dewatered sludge leads to a complex three-dimensional porous structure. Moreover, this operation is dependent on the way the material is processed. In this study, textural changes of sludge ... [more ▼] Drying dewatered sludge leads to a complex three-dimensional porous structure. Moreover, this operation is dependent on the way the material is processed. In this study, textural changes of sludge extrudates submitted to convective drying are followed by a 3D image analysis of reconstructed X-ray microtomograms. To achieve this goal, two different wastewater sludges collected in wastewater treatment plant after the thickening step and dewatered in the laboratory are used. It is showed that the evolution of the 3D-crack ratio vs. the residual water content evolves following a hyperbolic law. The 3D opening crack size distribution reveals two different types of pore development, i.e. a continuous pore size evolution for one sludge and the sudden appearance of cracks for the other sludge. [less ▲] Detailed reference viewed: 48 (3 ULg) Production of resorcinol formaldehyde xerogels by convective dryingLéonard, Angélique ; ; Crine, Michel ![]() in Proceedings of the joint conference of AFSIA (Association Française pour le Séchage dans l’Industrie et l’Agriculture) and Working group on Drying of EFCE at INA P-G, Paris, 12th and 13th May, 2005 (2005, May) Detailed reference viewed: 15 (0 ULg) Effect of back mixing during convective drying of wastewater sludgesLéonard, Angélique ; ; Salmon, Thierry et alin Proceeedings of the joint of AFSIA (Association Française de Séchage dans l'Industrie et l'Agriculture) and Working group on Drying of EFCE at INA P-G, Paris, 12th and 13th May, 2005 (2005, May) Detailed reference viewed: 11 (1 ULg) Moisture profiles determination during convective drying using x-ray microtomographyLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Canadian Journal of Chemical Engineering (2005), 83(1), 127-131 The knowledge of internal moisture profiles which develop during drying is essential for model validation purposes, but they are difficult to determine experimentally. This paper shows that X-ray ... [more ▼] The knowledge of internal moisture profiles which develop during drying is essential for model validation purposes, but they are difficult to determine experimentally. This paper shows that X-ray microtomography, together with image analysis, provides an accurate, non destructive and easy to use technique to determine moisture profiles. Results reported concern the drying of wastewater sludges whose management is becoming a real environmental challenge. An analysis of the development of moisture gradients at the sample external wall shows an influence of drying operating conditions. Finally, mass diffusion coefficients are estimated from the knowledge of both the moisture gradients and the drying flux. [less ▲] Detailed reference viewed: 38 (12 ULg) Mass transfer, mixing and gas hold-up in a circulating jet-loop nitrifying MBR; Salmon, Thierry ; Toye, Dominique et alin Proceedings of 7th World Congress of Chemical Enginnering - WCCE7, Glasgow, Scotland, 10-14 July 2005 (2005) Detailed reference viewed: 15 (1 ULg) Integrated adsorbent and process characterization. Application to air separation PSA processes; ; et al Conference (2005) Detailed reference viewed: 14 (2 ULg) Utilisation d’un nouveau tomographe à haute énergie pour extraire l’information structurale d’un échantillon de dévésiculeur; Toye, Dominique ; Marchot, Pierre et alPoster (2005) Detailed reference viewed: 9 (0 ULg) High energy, high resolution x-ray tomography applied to catalytic distillation packingsToye, Dominique ; ; Marchot, Pierre et alConference (2005) Detailed reference viewed: 8 (1 ULg) Transfert de matière gaz-liquide et mélange dans un réacteur membranaire à recirculation interne; Salmon, Thierry ; et alin Azzaro-Pantel, C.; Bertrand, J.; Cabassud, M. (Eds.) et al Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 81 (1 ULg) 3D imaging of reactive distillation packings with a new high energy x-ray tomographToye, Dominique ; ; Crine, Michel et alin Jong, A.; Takei, M.; William, R. A. (Eds.) et al Proceedings of 4th World Congress in Industrial Process Tomography (WCIPT4), Aizu, Japan, 5-8 septembre 2005 (2005) Detailed reference viewed: 24 (4 ULg) Evolution de l'écoulement de fluides non-newtoniens avec le temps d'agitation en cuve agitée par vélocimétrie par images de particules; Marchot, Pierre ; Toye, Dominique et alin SFGP (Ed.) Récents Progrès en Génie des procédés - N°92 - Le Génie des Procédés vers de nouveaux espaces, Actes du 10ème Congrès de la Société Française de Génie des Procédés, 20-22 septembre 2005, Toulouse, France (2005) Detailed reference viewed: 8 (4 ULg) Possibilities and limits of application of electrical resistance tomography in hydrodynamics of bubble columnsToye, Dominique ; ; Simon, Daniel et alin Canadian Journal of Chemical Engineering (2005), 83(1), 4-10 Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the ... [more ▼] Knowing the hydrodynamic regime in which is working a bubble column is of great importance because the regime affects strongly the mass transfer between the phases. To this end, we examine the potentialities of an Electrical Resistance Tomography (ERT) device. We analyse cross correlation of electrode pair measurements, of neighbouring pixels and power spectra of averaged pixels within a single plane as well as cross correlations of averaged pixels between two planes, without finding a clear signature of the churn turbulent flow. Variable gas flow rate inputs are used to determine the time resolution of the ERT. [less ▲] Detailed reference viewed: 32 (14 ULg) Convective drying of wastewater sludges: Influence of air temperature, superficial velocity, and humidity on the kineticsLéonard, Angélique ; Blacher, Silvia ; Marchot, Pierre et alin Drying Technology (2005), 23(8), 1667-1679 The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux ... [more ▼] The influence of air temperature, velocity, and humidity during convective drying of two different sludges (A and B) is investigated through a 3 3 factorial design. For sludge A, a constant drying flux period is observed, while sludge B is characterized by a long decreasing drying flux phase. A sensitivity analysis shows that temperature is the main operating parameter affecting the drying kinetics. Mass and heat transfer coefficients as well as water evaporation capacities are calculated from drying curves. Transfer coefficients are related to operating conditions through dimensionless relations. For both sludges, a linear relation is found between water evaporation capacity and the maximal measured drying flux. [less ▲] Detailed reference viewed: 56 (10 ULg) Wastewater sludge convective drying: Influence of sludge originLéonard, Angélique ; ; Salmon, Thierry et alin Environmental Technology (2004), 25(9), 1051-1057 This paper deals with thermal drying of wastewater sludges, whose management will become crucial in the forthcoming years. Sludges collected after mechanical dewatering in 5 different WWTPs are submitted ... [more ▼] This paper deals with thermal drying of wastewater sludges, whose management will become crucial in the forthcoming years. Sludges collected after mechanical dewatering in 5 different WWTPs are submitted to the same convective drying treatment in order to try finding some relations between the drying behaviours, the type of effluent and wastewater treatments. Results show clearly sludge drying remains a particularly complex operation because sludges may exhibit very different behaviours, both from kinetic and texture points of view. Initial moisture content and global composition are not sufficient to explain the different observed behaviours. It is too early to claim one or another type of water treatment has an influence on the drying behaviour. However, the drying rates can be classified in the inverse order of the organic content. Moreover for sludges at the same siccities, the harder the material (rheological properties), the higher the drying rate. Final textural properties can be related to the rheological properties and the internal diffusion limitations lowering the drying intensity. [less ▲] Detailed reference viewed: 72 (12 ULg) Image reconstruction in X-ray tomographyToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 13 (5 ULg) Computed Tomography at the University of Liège – Chemical Engineering LaboratoryToye, Dominique ; ; Léonard, Angélique et alScientific conference (2004, August) Detailed reference viewed: 9 (1 ULg) |
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